Sonochemical synthesis of Biginelli compounds

被引：0
|
作者：
M. S. Zhidovinova
O. V. Fedorova
G. L. Rusinov
I. G. Ovchinnikova
机构：
[1] Ural Branch of the Russian Academy of Sciences,Institute of Organic Synthesis
来源：
Russian Chemical Bulletin | 2003年 / 52卷
关键词：
Biginelli reactions; ethyl 4-R-6-methyl-2-oxo- and 4-R-6-methyl-2-thioxo-1,2,3,4-tetrahydropyrimidine-5-carboxylates; ultrasound effect;
D O I：
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中图分类号：
学科分类号：
摘要：
The ultrasound effect accelerates the Biginelli reaction 40 and more times. A sonochemical method for the synthesis of ethyl 4-R-6-methyl-2-oxo- and 4-R-6-methyl-2-thioxo-1,2,3,4-tetrahydropyrimidine-5-carboxylates was developed. The target products were obtained within 2 to 5 min in 90—95% yields.
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页码：2527 / 2528
页数：1
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