7-Bromo-5-phenyl-1,2-dihydro-3H-1,3,5-benztriazepin-2-one

被引：0
|
作者：
Vlasiuk S.V. [1 ]
Pavlovsky V.I. [1 ]
Andronati S.A. [1 ]
Gdaniec M. [2 ]
Simonov Yu.A. [3 ]
机构：
[1] A. V. Bogatsky Institute of Physical Chemistry, Ukraine National Academy of Sciences
[2] Mickiewicz University, Faculty of Chemistry
[3] Institute of Applied Physics, Moldavian Academy of Sciences
来源：
Chemistry of Heterocyclic Compounds | 2000年 / 36卷 / 9期
关键词：
Benztriazepine; Hydrogen bonds; IR spectroscopy; Semicarbazone of 2-aminobenzophenone; UV spectroscopy; X-ray crystallography;
D O I：
10.1023/A:1002790116884
中图分类号：
学科分类号：
摘要：
7-Bromo-5-phenyl-1,2-dihydro-3H-1,4-benztriazepin-2-one was obtained by thermolysis of the syn-4-phenylsemicarbazone of 2-aminobenzophenone. Its molecular and crystal structure were established by X-ray crystallography. The nature of the hydrogen bonds between molecules of the compound in solution and in the crystalline state was determined by IR spectroscopy and X-ray crystallography.
引用
收藏
页码：1077 / 1085
页数：8
相关论文
共 50 条
  • [31] Nootropic and Antihypoxic Properties of Novel Derivatives of 1,2-Dihydro-3H-1,4-Benzodiazepin-2-one
    S. A. Andronati
    T. L. Karaseva
    Ya. R. Krivenko
    V. I. Pavlovsky
    O. V Onufrienko
    A. A. Shandra
    Neurophysiology, 2017, 49 : 405 - 411
  • [32] Nootropic and Antihypoxic Properties of Novel Derivatives of 1,2-Dihydro-3H-1,4-Benzodiazepin-2-one
    Andronati, S. A.
    Karaseva, T. L.
    Krivenko, Ya. R.
    Pavlovsky, V. I.
    Onufrienko, O. V.
    Shandra, A. A.
    NEUROPHYSIOLOGY, 2017, 49 (06) : 405 - 411
  • [33] Molecular and crystal structure of 1,2-dihydro-3H-1,3,4-benzotriazepines
    Chumakov Yu.M.
    Simonov Yu.A.
    Bocelli G.
    Gdaniec M.
    Vlassiuk S.V.
    Pavlovsky V.I.
    Chemistry of Heterocyclic Compounds, 2006, 42 (7) : 907 - 913
  • [34] AN ANOMALOUS REACTION OF 7-CHLORO-2-HYDRAZONO-5-PHENYL-1,2-DIHYDRO-3H-1,4-BENZODIAZEPINE WITH SODIUM-ACETATE AND 1,1'-CARBONYLDIIMIDAZOLE
    BANKS, WR
    HAWI, AA
    DIGENIS, GA
    JOURNAL OF HETEROCYCLIC CHEMISTRY, 1991, 28 (02) : 533 - 535
  • [35] PREPARATION OF 3,5-DIMETHYL-2-THIOXO-1,2-DIHYDRO-3H-1,3,4-BENZOTRIAZEPINES
    MORGENSTERN, O
    RICHTER, P
    PHARMAZIE, 1985, 40 (10): : 694 - 696
  • [36] 5-tert-butyl-4-bromo-1,2-dihydro-1H-pyrazol-3(2H)-one monohydrate
    Lynch, DE
    McClenaghan, I
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2005, 61 : O2349 - O2351
  • [37] 1,4-BENZODIAZEPINES, THEIR CYCLIC HOMOLOGS AND ANALOGS .30. SYNTHESIS AND PROPERTIES OF 3 AND 7-AMINO-5-PHENYL-1,2-DIHYDRO-3H-1,4-BENZDIAZEPINE-2-ONES
    ZHILINA, ZI
    BOGATSKII, AV
    ANDRONATI, SA
    DANILINA, NI
    KHIMIYA GETEROTSIKLICHESKIKH SOEDINENII, 1979, (04): : 545 - 549
  • [38] SPATIAL STRUCTURE OF 1,2-DIHYDRO-3H-1,4-BENZDIAZEPIN-2-ONES
    ANDRONATI, SA
    PROKOPENKO, IA
    YAVORSKY, AS
    KHVOSTENKO, OG
    BOLDESKUL, IE
    DOPOVIDI AKADEMII NAUK UKRAINSKOI RSR SERIYA B-GEOLOGICHNI KHIMICHNI TA BIOLOGICHNI NAUKI, 1988, (01): : 32 - 34
  • [39] Synthesis and Analgesic Activity of 3-Arylamino-1,2-Dihydro-3H-1,4-Benzodiazepin-2-Ones
    V. I. Pavlovskii
    I. Yu. Ushakov
    T. A. Kabanova
    E. I. Khalimova
    V. Kh. Kravtsov
    S. A. Andronati
    Pharmaceutical Chemistry Journal, 2015, 49 : 592 - 597
  • [40] Molecular and crystalline structure of 1,2-dihydro-3H-1,3,4-benzotriazepine derivatives
    Chumakov, Yu. M.
    Simonov, Yu. A.
    Bocelli, G.
    Gdaniec, M.
    Vlasiuk, S. V.
    Pavlovsky, V. I.
    KHIMIYA GETEROTSIKLICHESKIKH SOEDINENII, 2006, (07): : 1048 - 1056
12345