7-Bromo-5-phenyl-1,2-dihydro-3H-1,3,5-benztriazepin-2-one

被引：0
|
作者：
Vlasiuk S.V. [1 ]
Pavlovsky V.I. [1 ]
Andronati S.A. [1 ]
Gdaniec M. [2 ]
Simonov Yu.A. [3 ]
机构：
[1] A. V. Bogatsky Institute of Physical Chemistry, Ukraine National Academy of Sciences
[2] Mickiewicz University, Faculty of Chemistry
[3] Institute of Applied Physics, Moldavian Academy of Sciences
来源：
Chemistry of Heterocyclic Compounds | 2000年 / 36卷 / 9期
关键词：
Benztriazepine; Hydrogen bonds; IR spectroscopy; Semicarbazone of 2-aminobenzophenone; UV spectroscopy; X-ray crystallography;
D O I：
10.1023/A:1002790116884
中图分类号：
学科分类号：
摘要：
7-Bromo-5-phenyl-1,2-dihydro-3H-1,4-benztriazepin-2-one was obtained by thermolysis of the syn-4-phenylsemicarbazone of 2-aminobenzophenone. Its molecular and crystal structure were established by X-ray crystallography. The nature of the hydrogen bonds between molecules of the compound in solution and in the crystalline state was determined by IR spectroscopy and X-ray crystallography.
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页码：1077 / 1085
页数：8
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