Numerical optimization of hydrothermal liquefaction process for the production of bio-oil and bio-char from Citrus maxima peel waste and product characterization

被引:0
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作者
Afzal Hussain
Sanjay Kumar
Fohad Mabood Husain
Vinod Kumar
Mikhail S. Vlaskin
Mohamed F. Alajmi
机构
[1] King Saud University,Department of Pharmacognosy, College of Pharmacy
[2] Department of Food Science and Technology,Department of Food Science and Nutrition, College of Food and Agriculture Sciences
[3] Graphic Era (Deemed to Be University),Peoples’ Friendship
[4] King Saud University,undefined
[5] University of Russia,undefined
[6] (RUDN University),undefined
[7] Joint Institute for High Temperatures of the Russian Academy of Sciences,undefined
关键词
Response surface; Central composite design; Pomelo peel; Nuclear magnetic resonance; Design expert; Response surface;
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中图分类号
学科分类号
摘要
This research study aims to potential utilization of Citrus maxima peel waste and optimize the hydrothermal liquefaction process for the production of bio-oil (BO) and bio-char (BC). The effect of several HTL processing variables on BO yield (%) and BC yield (%), including temperature, retention period, and slurry concentration, has been examined using central composite design (CCD) (a three-level three-factor design). The optimized values of HTL process variables were found to be 240 °C (temperature), 52 min (retention time), and 7% (slurry concentration) and the corresponding responses were 5.794% (BO yield) and 29.450% (BC yield). The values obtained from the RSM-CCD model as the predicted values agreed with the experimental values (5.93% and 30.14%). Further the BO and BC obtained under optimized conditions and CPP were analyzed to identify the variations by 1H-NMR, GC–MS, FT-IR, and CHNO-S.
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页码:102462 / 102473
页数:11
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