Determination of Polycyclic Aromatic Hydrocarbons in Seafood

被引：0
|
作者：
C. M. Taylor
J. M. Raines
J. M. Rodriguez
机构：
[1] Shimadzu,Department of Biochemistry and Molecular Biology
[2] Mississippi State Chemical Laboratory,undefined
[3] Mississippi State University,undefined
来源：
Food Analytical Methods | 2013年 / 6卷
关键词：
Comprehensive two-dimensional gas chromatography-quadrupole mass spectrometry (GCXGC-MS); Polycyclic aromatic hydrocarbons (PAHs); Selective ion monitoring (SIM); Seafood; High-pressure liquid chromatography fluorescence detector (HPLC-FL); Bland–Altman analysis;
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学科分类号：
摘要：
The aim of this project is to determine polycyclic aromatic hydrocarbons (PAHs) in several seafood matrices, i.e., fish, and mussel, by the use of comprehensive two-dimensional gas chromatography-quadrupole mass spectrometry (GCXGC-MS). The procedure involves a simple extraction of PAHs, a filtration and concentration step followed by GCXGC-MS analysis. PAHs were determined in fish tissue samples by GCXGC-MS and by a standard high-pressure liquid chromatography fluorescence detector method. A Bland–Altman analysis of the two methods was performed. It indicated equivalence between the two methods. Analysis of mussel tissue (National Institute of Standards and Technology (NIST)-SRM 2974a) was performed. The results were in line with the official results of NIST.
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页码：1330 / 1336
页数：6
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