Crystal structure of bis 4-benzyl piperidinium monohydrogenmonophosphate pentahydrate, [C6H5CH2CHCH2CH2NH2CH2CH2]2HPO4·5H2O

被引：0

作者：

Z. Elaoud

S. Kamoun

T. Mhiri

A. Daoud

A. Driss

机构：

[1] ENIS,Laboratoire de Cristallochimie du Solide

[2] Laboratoire de l'Etat Solide,Laboratoire de Cristallochimie, Département de Chimie, Faculté des Sciences de Tunis

[3] Département de Chimie,undefined

[4] Faculté,undefined

[5] Campus Universitaire,undefined

来源：

Journal of Chemical Crystallography | 2004年 / 34卷

关键词：

Organic phosphate; structure;

D O I：

暂无

中图分类号：

学科分类号：

摘要：

The salt bis 4-benzyl piperidinium monohydrogenmonophosphate pentahydrate is orthorhombic with the following unit cell dimensions: a = 11.235(2) Å, b = 27.924(6) Å, c = 9.321(4) Å space group Pca21 with Z = 4. The structure was solved by the Patterson method and refined to final R value of 0.049 for 1802 independent reflections. The flack parameter is 0.14 with an e.s.d. of 0.23. The structure consists of infinite parallel two-dimensional [110] planes built of mutually connected ions and water molecules by strong O—H,...,O and N—H,...,O hydrogen bonding. There are no contacts other than normal van der Waals interactions between the layers.

引用

页码：337 / 341

页数：4

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