Sonochemistry as a General Procedure for the Synthesis of Coumarins, Including Multigram Synthesis

被引：35

作者：

da Silveira Pinto, Ligia S. ^{[1
]}

de Souza, Marcus V. N. ^{[1
,2
]}

机构：

[1] Univ Fed Rio de Janeiro, Inst Quim, Dept Quim Organ, CP 68563, BR-21945970 Rio De Janeiro, Brazil

[2] FioCruz Fundacao Oswaldo Cruz, Inst Tecnol Farmacos Far Manguinhos, Rua Sizenando Nabuco 100, BR-21041250 Manguinho, RJ, Brazil

来源：

SYNTHESIS-STUTTGART | 2017年 / 49卷 / 12期

关键词：

coumarins; sonochemistry; synthesis; multigram scale; smaller scale; ULTRASONIC ASSISTED SYNTHESIS; KNOEVENAGEL; DERIVATIVES;

D O I：

10.1055/s-0036-1590201

中图分类号：

O62 [有机化学];

学科分类号：

070303 ; 081704 ;

摘要：

This study describes a general procedure for the synthesis of different coumarins via sonochemistry using active methylene compounds and 2-hydroxybenzaldehydes or resorcinol. The application of sonochemistry for the synthesis of these compounds was also very effective on a multigram scale with a higher yield, higher amount of crystalline compound, and shorter reaction time compared with the compounds obtained using the classical procedures.

引用

页码：2677 / 2682

页数：6

共 50 条

[21] Multigram Synthesis of Pure HMF and BHMF
Arico, Fabio
Trapasso, Giacomo
Mazzi, Giovanna
Chicharo, Beatriz
Annatelli, Mattia
Dalla Torre, Davide
ORGANIC PROCESS RESEARCH & DEVELOPMENT, 2022, 26 (10) : 2830 - 2838
[22] Multigram Synthesis of Thallium Trispyrazolylborate Compounds
Olmos, Andrea
Pereira, Ana
Belderrain, Tomas R.
Perez, Pedro J.
SYNTHESIS-STUTTGART, 2018, 50 (17): : 3333 - 3336
[23] An improved multigram synthesis of tetradeuterated buspirone
Vashishtha, SC
McKay, G
Midha, KK
JOURNAL OF LABELLED COMPOUNDS & RADIOPHARMACEUTICALS, 1999, 42 (10): : 919 - 925
[24] An Efficient Multigram Synthesis of Alkannin and Shikonin
Wang, Rubing
Zhou, Shanshan
Jiang, Hudagula
Zheng, Xiaogang
Zhou, Wen
Li, Shaoshun
EUROPEAN JOURNAL OF ORGANIC CHEMISTRY, 2012, 2012 (07) : 1373 - 1379
[25] Multigram Synthesis of Functionalized Spirocyclic Diazirines
Martyloga, Oleksandr V.
Myronenko, Artamon
Tkachenko, Anton M.
Matvienko, Vitalii O.
Kuchkovska, Yuliya O.
Grygorenko, Oleksandr O.
EUROPEAN JOURNAL OF ORGANIC CHEMISTRY, 2019, 2019 (23) : 3744 - 3750
[26] Multigram scale synthesis of spirocyclic pyrrolidines
Ryabukhin, Sergey
Volochnyuk, Dmitriy
Melnykov, Konstantyn
Ostapchuk, Eugeniy
ABSTRACTS OF PAPERS OF THE AMERICAN CHEMICAL SOCIETY, 2019, 257
[27] A facile, multigram synthesis of ribofuranoid glycals
Walker, JA
Chen, JJ
Wise, DS
Townsend, LB
JOURNAL OF ORGANIC CHEMISTRY, 1996, 61 (06): : 2219 - 2221
[28] Synthesis of Functionalized Coumarins
Shaabani, Ahmad
Ghadari, Rahim
Rezayan, Ali Hossein
IRANIAN JOURNAL OF CHEMISTRY & CHEMICAL ENGINEERING-INTERNATIONAL ENGLISH EDITION, 2011, 30 (04): : 19 - 22
[29] Materials synthesis using sonochemistry.
Suslick, KS
Fang, MM
Hyeon, T
Ries, J
ABSTRACTS OF PAPERS OF THE AMERICAN CHEMICAL SOCIETY, 1996, 211 : 267 - INOR
[30] NEW SYNTHESIS OF COUMARINS
CHATTERJEE, A
BHATTACHARYA, S
BANERJI, J
GHOSH, PC
INDIAN JOURNAL OF CHEMISTRY SECTION B-ORGANIC CHEMISTRY INCLUDING MEDICINAL CHEMISTRY, 1977, 15 (03): : 214 - 216

← 1 2 3 4 5 →