3-[(4-Bromoanilino)carbonyl]prop-2-enoic acid

被引:4
|
作者
Parvez, M
Shahid, K
Shahzadi, S
Ali, S
机构
[1] Univ Calgary, Dept Chem, Calgary, AB T2N 1N4, Canada
[2] Quaid I Azam Univ, Dept Chem, Islamabad 45320, Pakistan
关键词
D O I
10.1107/S1600536804026029
中图分类号
O7 [晶体学];
学科分类号
0702 ; 070205 ; 0703 ; 080501 ;
摘要
The crystal structure of the title compound, C10H8BrNO3, establishes that condensation of 4-bromoaniline with maleic anhydride gives the title compound at room temperature. There are strong intermolecular N-H...O hydrogen bonds [N...O = 2.814 (3) Angstrom and 2.817 (3) Angstrom] linking the molecules into sheets lying parallel to the bc plane. The carboxyl groups adopt an anti-planar conformation and participate in intramolecular O-H...O hydrogen bonds [O...O = 2.484 (3) and 2.487 (3) Angstrom]. There are two molecules in the asymmetric unit.
引用
收藏
页码:O2079 / O2081
页数:3
相关论文
共 50 条
  • [31] (E)-3-(4-Chlorophenyl)-2-phenylprop-2-enoic acid
    Sadiq-ur-Rehman
    Ali, Saqib
    Shahzadi, Saira
    Parvez, Masood
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2009, 65 : 01562 - U2371
  • [32] Crystal structure, Hirshfeld surfaces and DFT computation of NLO active (2E)-2-(ethoxycarbonyl)-3-[(1-methoxy-1-oxo-3-phenylpropan-2-yl)amino] prop-2-enoic acid
    Venkatesan, Perumal
    Thamotharan, Subbiah
    Ilangovan, Andivelu
    Liang, Hongze
    Sundius, Tom
    SPECTROCHIMICA ACTA PART A-MOLECULAR AND BIOMOLECULAR SPECTROSCOPY, 2016, 153 : 625 - 636
  • [33] Synthesis and Characterization of Organic 2-(Cyano 3-(4-Diphenylamino) Phenyl) Prop 2-Enoic Acid Dye for Electrochemical Cell Applications
    Shanmugam, Kotteswaran
    Pandian, Senthil M.
    Ramasamy, P.
    DAE SOLID STATE PHYSICS SYMPOSIUM 2018, 2019, 2115
  • [34] INVESTIGATION OF THE ELECTRONIC-STRUCTURE OF 2-(ACETYLAMINO)PROP-2-ENOIC ACID (N-ACETYLDEHYDROALANINE) BY HEI AND HEII PHOTOELECTRON-SPECTROSCOPY
    AJO, D
    GRANOZZI, G
    CILIBERTO, E
    FRAGALA, I
    JOURNAL OF THE CHEMICAL SOCIETY-PERKIN TRANSACTIONS 2, 1980, (03): : 483 - 485
  • [35] Molecular conformational analysis, vibrational spectra, NBO analysis and first hyperpolarizability of (2E)-3-(3-chlorophenyl)prop-2-enoic anhydride based on density functional theory calculations
    Mary, Y. Sheena
    Raju, K.
    Panicker, C. Yohannan
    Al-Saadi, Abdulaziz A.
    Thiemann, Thies
    SPECTROCHIMICA ACTA PART A-MOLECULAR AND BIOMOLECULAR SPECTROSCOPY, 2014, 131 : 471 - 483
  • [36] (E)-3-(3-phenylpropoxy)but-2-enoic acid
    Li, J
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2006, 62 : O1994 - O1995
  • [37] Synthesis of 2-Cyano 3-(4 dimethylaminophenyl) prop 2-enoic acid dye derived from 4-dimethy laminobenzaldehyde and methyl cyanoacetate and its properties
    Kotteswaran S.
    Pandian M.S.
    Ramasamy P.
    Materials Research Innovations, 2016, 20 (02) : 112 - 116
  • [38] 2-Cyano-3-(2,3,6,7-tetrahydro-1H,5Hbenzo[ij]quinolizin-9-yl)prop-2-enoic acid dimethyl sulfoxide monosolvate
    Yennawar, Hemant
    He, Gang
    Rumble, Christopher
    Maroncelli, Mark
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2012, 68 : O3204 - +
  • [39] Utility of p-Acetamidobenzoyl Prop-2-enoic Acid in the Synthesis of New alpha-Amino Acids and Using Them as Building Blocks in Heterocyclic Synthesis
    El-Hashash, M. A.
    Rizk, S. A.
    Aburzeza, M. M.
    EGYPTIAN JOURNAL OF CHEMISTRY, 2011, 54 (03): : 299 - 312
  • [40] Methyl 4-(4-bromoanilino)-2 ',5-dioxo-5H-spiro[furan-2,3 '-indoline]-3-carboxylate
    Gangadharan, Rajeswari
    Kiruthika, Selvarangam E.
    Sethusankar, K.
    Perumal, P. T.
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2014, 70 : 0210 - +