Efficient synthesis of N,N′-methylenebisglycolurils

被引:7
|
作者
Kravchenko, Angelina N. [1 ]
Chikunov, Ilya E. [1 ]
Gazieva, Galina A. [1 ]
Makhova, Nina N. [1 ]
机构
[1] Russian Acad Sci, ND Zelinskii Organ Chem Inst, Moscow 119991, Russia
关键词
D O I
10.1016/j.mencom.2016.03.018
中图分类号
O6 [化学];
学科分类号
0703 ;
摘要
Coupling of 6-(carboxy)alkyl-2,4-dialkylglycolurils with N-(hydroxymethyl)glycolurils gives N,N'-methylenebisglycolurils totally substituted at the nitrogen atoms, which are formed mostly as racemate diastereomers.
引用
收藏
页码:136 / 138
页数:3
相关论文
共 50 条
  • [31] Boric acid catalyzed efficient synthesis of symmetrical N,N′-alkylidene bisamides
    G. Harichandran
    S. David Amalraj
    P. Shanmugam
    Journal of the Iranian Chemical Society, 2011, 8 : 298 - 305
  • [32] An efficient and greener protocol towards synthesis of unsymmetrical N,N′-biphenyl urea
    Mane, Madhav
    Balaskar, Ravi
    Gavade, Sandip
    Pabrekar, Pramod
    Mane, Dhananjay
    ARABIAN JOURNAL OF CHEMISTRY, 2013, 6 (04) : 423 - 427
  • [33] A facile and efficient synthesis of N,N-dimethylarylamines from aryl bromides
    Zhao, JK
    Wang, YG
    CHINESE CHEMICAL LETTERS, 2002, 13 (12) : 1149 - 1151
  • [34] A Facile and Efficient Synthesis of N,N-Dimethylarylamines from Aryl Bromides
    Jian Kui ZHAO
    Chinese Chemical Letters, 2002, (12) : 1149 - 1151
  • [35] Efficient Enantioselective Synthesis of Dihydropyrans Using a Chiral N,N′-Dioxide as Organocatalyst
    Feng, Juhua
    Fu, Xuan
    Chen, Zhenling
    Lin, Lili
    Liu, Xiaohua
    Feng, Xiaoming
    ORGANIC LETTERS, 2013, 15 (11) : 2640 - 2643
  • [36] An Efficient Solventless Method for the Synthesis of N,N-Dialkyl Sulfonamide Derivatives
    Zare, A.
    Hasaninejad, A.
    Zare, A. R. Moosavi
    Khalafi-Nezhad, A.
    Parhami, A.
    JOURNAL OF THE IRANIAN CHEMICAL SOCIETY, 2008, 5 (04) : 617 - 622
  • [37] Boric acid Catalyzed Efficient Synthesis of Symmetrical N,N′-Alkylidene Bisamides
    Harichandran, G.
    Amalraj, S. David
    Shanmugam, P.
    JOURNAL OF THE IRANIAN CHEMICAL SOCIETY, 2011, 8 (01) : 298 - 305
  • [38] Nitrene-mediated intermolecular N–N coupling for efficient synthesis of hydrazides
    Hao Wang
    Hoimin Jung
    Fangfang Song
    Shiyang Zhu
    Ziqian Bai
    Danye Chen
    Gang He
    Sukbok Chang
    Gong Chen
    Nature Chemistry, 2021, 13 : 378 - 385
  • [39] Cheap, Efficient, and Scalable Synthesis of 4-N,N-Dimethylaminopiperidine
    Diwan, Sachin S.
    Dalvi, Sonali W.
    Mulla, Hormuzd R.
    SYNTHETIC COMMUNICATIONS, 2009, 39 (02) : 273 - 277
  • [40] A SIMPLE AND EFFICIENT SYNTHESIS OF LACTONE N,N-DIALKYLHYDRAZONES AND THEIR ISOMERIC N-(DIALKYLAMINO)-LACTAMS
    ENDERS, D
    BRAUERSCHEIB, S
    FEY, P
    SYNTHESIS-STUTTGART, 1985, (04): : 393 - 396