Tetraphenyltetrabenzoporphyrinates of Ni(II), Pd(II), Pt(II) and Pt(IV)

被引：4

作者：

Maltceva, Olga V. ^{[1
]}

Chizhova, Natalya V. ^{[1
]}

Kumeev, Roman S. ^{[1
]}

Mamardashvili, Nugzar Zh. ^{[1
]}

机构：

[1] Russian Acad Sci, GA Krestov Inst Solut Chem, Ivanovo 153045, Russia

来源：

MACROHETEROCYCLES | 2017年 / 10卷 / 01期

关键词：

Synthesis; tetraphenyltetrabenzoporphyrinate; H-1 NMR spectroscopy; electron absorption spectroscopy; mass-spectrometry; elemental analysis; COMPLEXES; TETRABENZOPORPHYRINS;

D O I：

10.6060/mhc160541c

中图分类号：

O6 [化学];

学科分类号：

0703 ;

摘要：

The metal exchange reaction of 5,10,15,20-tetraphenyltetrabenzoporphyrinate of Cd(II) with Ni(II), Pd(II) and Pt(II) chlorides in DMF and phenol was investigated. Corresponding porphyrinates of Ni(II), Pd(II) and Pt(II) were obtained. 5,10,15,20-Tetraphenyltetrabenzoporphyrinate Pt(IV)(Br)(2) was synthesized through direct addition of Br 2 to the porphyrinate Pt(II) in chloroform. The prepared compounds were identified by the methods of electronic absorption, H-1 NMR spectroscopy, mass spectrometry and elemental analysis.

引用

页码：68 / 71

页数：4

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