Synthesis of Crown Compounds Containing a 1,3,4-Oxadiazole Moiety: Microwave-Assisted Synthesis

被引：3

作者：

Outirite, Moha ^{[1
]}

Lebrini, Mounim ^{[1
]}

Lagrenee, Michel ^{[1
]}

Bentiss, Fouad ^{[2
]}

机构：

[1] ENSCL, Unite Catalyse & Chim Solide, CNRS, UMR 8181, F-59652 Villeneuve Dascq, France

[2] Univ Chouaib Doukkali, Fac Sci, Lab Chim Coordinat & Analyt, M-24000 El Jadida, Morocco

来源：

JOURNAL OF HETEROCYCLIC CHEMISTRY | 2010年 / 47卷 / 03期

关键词：

TRIAZOLE SUBCYCLIC UNIT; MACROCYCLIC POLYETHER; 1,3,4-THIADIAZOLE MOIETY; COMPLEXATION PROPERTIES; LIGANDS;

D O I：

10.1002/jhet.201

中图分类号：

O62 [有机化学];

学科分类号：

070303 ; 081704 ;

摘要：

New macrocyclic polyether compounds containing a 2,5-bis(2-hydroxypheny1)-1,3,4-oxadiazole moiety are quickly prepared by a nucleophilic substitution reaction involving ethylene glycol ditosylate or polyethylene glycol ditosylate and a biphenol, the 2,5-bis(2-hydroxyphenyl)-1,34-oxadiazole, with solid anhydrous potassium carbonate as a base under microwave irradiation (monomode and multimode). The structures of new macrocyclic polyether compounds were confirmed by (1)H, (13)C NMR, mass spectrometry, and elemental analysis.

引用

页码：555 / 557

页数：3

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