Synthesis of Crown Compounds Containing a 1,3,4-Oxadiazole Moiety: Microwave-Assisted Synthesis

被引:3
|
作者
Outirite, Moha [1 ]
Lebrini, Mounim [1 ]
Lagrenee, Michel [1 ]
Bentiss, Fouad [2 ]
机构
[1] ENSCL, Unite Catalyse & Chim Solide, CNRS, UMR 8181, F-59652 Villeneuve Dascq, France
[2] Univ Chouaib Doukkali, Fac Sci, Lab Chim Coordinat & Analyt, M-24000 El Jadida, Morocco
关键词
TRIAZOLE SUBCYCLIC UNIT; MACROCYCLIC POLYETHER; 1,3,4-THIADIAZOLE MOIETY; COMPLEXATION PROPERTIES; LIGANDS;
D O I
10.1002/jhet.201
中图分类号
O62 [有机化学];
学科分类号
070303 ; 081704 ;
摘要
New macrocyclic polyether compounds containing a 2,5-bis(2-hydroxypheny1)-1,3,4-oxadiazole moiety are quickly prepared by a nucleophilic substitution reaction involving ethylene glycol ditosylate or polyethylene glycol ditosylate and a biphenol, the 2,5-bis(2-hydroxyphenyl)-1,34-oxadiazole, with solid anhydrous potassium carbonate as a base under microwave irradiation (monomode and multimode). The structures of new macrocyclic polyether compounds were confirmed by (1)H, (13)C NMR, mass spectrometry, and elemental analysis.
引用
收藏
页码:555 / 557
页数:3
相关论文
共 50 条
  • [1] MICROWAVE-ASSISTED SYNTHESIS OF SOME NOVEL BENZIMIDAZOLE COMPOUNDS CONTAINING OXADIAZOLE MOIETY
    Kahveci, Bahittin
    Sosan, Nesibe
    Mentese, Emre
    Yilmaz, Fatih
    REVUE ROUMAINE DE CHIMIE, 2013, 58 (06) : 511 - 515
  • [2] Synthesis and pesticidal activity of new 1,3,4-oxadiazole thioether compounds containing a trifluoromethylpyrazoyl moiety
    Shi, Hai-Bo
    Zhai, Zhi-Wen
    Min, Li-Jing
    Han, Liang
    Sun, Na-Bo
    Cantrell, Charles L.
    Bajsa-Hirschel, Joanna
    Duke, Stephen O.
    Liu, Xing-Hai
    RESEARCH ON CHEMICAL INTERMEDIATES, 2022, 48 (11) : 4753 - 4767
  • [3] Synthesis and pesticidal activity of new 1,3,4-oxadiazole thioether compounds containing a trifluoromethylpyrazoyl moiety
    Hai-Bo Shi
    Zhi-Wen Zhai
    Li-Jing Min
    Liang Han
    Na-Bo Sun
    Charles L. Cantrell
    Joanna Bajsa-Hirschel
    Stephen O. Duke
    Xing-Hai Liu
    Research on Chemical Intermediates, 2022, 48 : 4753 - 4767
  • [4] Synthesis and Antimicrobial Properties of 1,3,4-Oxadiazole Analogs Containing Dibenzosuberane Moiety
    Moger, Manjunath
    Satam, Vijay
    Govindaraju, Darshan Raj C.
    Paniraj, A. S.
    Gopinath, Vadiraj S.
    Hindupur, Rama Mohan
    Pati, Hari N.
    JOURNAL OF THE BRAZILIAN CHEMICAL SOCIETY, 2014, 25 (01) : 104 - 111
  • [5] Synthesis and Biological Activities of Novel Cyanoacrylates Containing 1,3,4-Oxadiazole Moiety
    Shi, Yujn
    Li, Yang
    Fang, Yuan
    Chen, Jia
    Ye, Linyu
    Ge, Shushan
    Dai, Hong
    CHINESE JOURNAL OF ORGANIC CHEMISTRY, 2016, 36 (10) : 2472 - 2478
  • [6] Synthesis and Bioactivities of Novel 1,3,4-oxadiazole Derivatives Containing Pyridine Moiety
    Sun, Guo-Xiang
    Shi, Yan-Xia
    Sun, Zhao-Hui
    Yang, Ming-Yan
    Wu, Hong-Ke
    Weng, Jian-Quan
    Tan, Cheng-Xia
    Liu, Xing-Hai
    Li, Bao-Ju
    Zhang, Yong-Gang
    LETTERS IN DRUG DESIGN & DISCOVERY, 2014, 11 (09) : 1119 - 1123
  • [7] Synthesis and Fungicidal Activity of 1,3,4-Oxadiazole Derivatives Containing Pyrazole Moiety
    Sun, Nabo
    Tong, Jianying
    Wu, Hongke
    CHINESE JOURNAL OF ORGANIC CHEMISTRY, 2013, 33 (01) : 101 - 105
  • [8] Microwave-assisted synthesis of benzimidazole bearing 1,3,4-oxadiazole derivatives: screening for their in vitro antimicrobial activity
    Desai, N. C.
    Kotadiya, G. M.
    MEDICINAL CHEMISTRY RESEARCH, 2014, 23 (09) : 4021 - 4033
  • [9] Design and Microwave-assisted Synthesis of 1,3,4-Oxadiazole Derivatives for Analgesic and Anti-inflammatory Activity
    Biju, C. R.
    Ilango, K.
    Prathap, Manju
    Rekha, K.
    JOURNAL OF YOUNG PHARMACISTS, 2012, 4 (01) : 33 - 37
  • [10] Microwave-Assisted Synthesis and Molecular Docking Studies of Fluorinated 1,3,4-Oxadiazole Derivatives as Antimicrobial Agent
    Dhotre, B. K.
    Patharia, M. A.
    Khandebharad, A. U.
    Raut, S., V
    Pathan, M. A.
    RUSSIAN JOURNAL OF BIOORGANIC CHEMISTRY, 2020, 46 (06) : 1110 - 1116