Sintering, physicomechanical, thermal expansion and microstructure properties of cordierite ceramics based on utilizing silica fume waste

被引:21
|
作者
Khattab, R. M. [1 ]
Abo-Almaged, H. H. [1 ]
Ajiba, N. A. [1 ]
Badr, H. A. [1 ]
Gaber, A. A. [1 ]
Taha, M. A. [2 ]
Sadek, H. E. H. [1 ]
机构
[1] Natl Res Ctr, Refractories Ceram & Bldg Mat Dept, Cairo 12622, Egypt
[2] Natl Res Ctr NRC, Solid State Phys Dept, Cairo 12622, Egypt
关键词
Cordierite; Fumed silica; Electrical properties; Thermal properties; Mechanical properties; IN-SITU FORMATION; MECHANICAL-PROPERTIES; ELECTRICAL-PROPERTIES; COMPOSITE; TALC; TEMPERATURE; BEHAVIOR; MULLITE; POWDERS; CRYSTALLIZATION;
D O I
10.1016/j.matchemphys.2021.124829
中图分类号
T [工业技术];
学科分类号
08 ;
摘要
In the present work, cordierite ceramics are prepared through the solid reaction method using calcined alumina, silica fume, and talc as starting materials. Pressed samples and powders are sintered and calcined at various temperatures; 1300, 1350 and 1400 degrees C. The particle size, phase composition and morphology of the raw materials, and the calcined and sintered cordierite samples are analyzed. The physical properties, surface area, DSC, TG, thermal expansion and electrical and mechanical properties of the cordierite samples are also studied. In addition, the physical, thermal, mechanical, and electrical properties are investigated under the effect of heat treatment. The results indicated that 1350 degrees C is the optimum sintering temperature with 10.323% apparent porosity and 2.112 g/cm(3) bulk density and the crystallization of the cordierite ceramic was crack-free and has low thermal expansion. It also, showed good dielectrical constant of 5.5 and good mechanical properties such as 2.71 MPa m0.5 fracture toughness and 5.38 GPa micro hardness.
引用
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页数:10
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