Synthesis and crystal structure of one new Pb(II) complex constructed by 1,10-phenanthroline and two carboxylate ligands

被引：7
|
作者：
Zhang, Lu-Lin [1 ]
Tang, Shi-Li [1 ]
Li, De-Jun [1 ]
Cheng, Yuan-Zheng [1 ]
Zhang, Li-Ping [1 ]
机构：
[1] Weifang Med Univ, Sch Pharm, Weifang 261053, Peoples R China
来源：
MAIN GROUP METAL CHEMISTRY | 2021年 / 44卷 / 01期
关键词：
lead(II); 1,10-phenanthroline; 4-nitrobenzoate; acetate; crystal structure; COORDINATION POLYMERS; LONE-PAIR; LEAD(II) COMPLEXES; HYDROTHERMAL SYNTHESIS; ORGANIC FRAMEWORKS; ACID; ARCHITECTURES; PB; LUMINESCENCE; DIVERSITY;
D O I：
10.1515/mgmc-2021-0019
中图分类号：
O61 [无机化学];
学科分类号：
070301 ; 081704 ;
摘要：
The complex [Pb(phen)(4-NB)(CH3COO)] of lead(II) was prepared and characterized by means of elemental analysis, FT-IR, and single crystal X-ray analysis, where phen = 1,10-phenanthroline, 4-NB = 4-nitrobenzoate. The single crystal X-ray analysis indicates that the complex is a monomeric species, including two carboxylate ligands, and adopts a hemidirected structure. It is further extended by intermolecular C-H center dot center dot center dot O hydrogen bonds, p-p interactions and secondary Pb center dot center dot center dot O interactions to form two-dimensional supramolecular architecture.
引用
收藏
页码：157 / 164
页数：8
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