9-(4-Hydroxy-3-methoxyphenyl)-3,3,6,6-tetramethyl-3,4,5,6-tetrahydro-9H-xanthene-1,8(2H,7H)-dione

被引:2
|
作者
Hasanudin, Noorhafizah [2 ]
Rahim, Aisyah Saad Abdul [2 ]
Mohamed, Nornisah [2 ]
Quah, Ching Kheng [1 ]
Fun, Hoong-Kun [1 ]
机构
[1] Univ Sains Malaysia, Sch Phys, Xray Crystallog Unit, Usm 11800, Penang, Malaysia
[2] Univ Sains Malaysia, Sch Pharmaceut Sci, Usm 11800, Penang, Malaysia
来源
ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE | 2010年 / 66卷
关键词
X-RAY; DERIVATIVES;
D O I
10.1107/S1600536810020258
中图分类号
O7 [晶体学];
学科分类号
0702 ; 070205 ; 0703 ; 080501 ;
摘要
In the title compound, C24H28O5, the two cyclohexene rings adopt envelope conformations, and the planes through the coplanar atoms makes dihedral angles of 82.86 (6) and 77.90 (6)degrees with the benzene ring. The two cyclohexene rings make a dihedral angle of 5.33 (6)degrees between their least-squares planes. The pyran ring adopts a flattened boat conformation. In the crystal packing, molecules are linked into two-dimensional networks parallel to the ab plane via O-H center dot center dot center dot O and C-H center dot center dot center dot O interactions.
引用
收藏
页码:O1538 / U288
页数:13
相关论文
共 50 条
  • [21] 10-(2-Fluorophenyl)-9-(4-methoxyphenyl)-3,3,6,6-tetramethyl-3,4,6,7-tetrahydroacridine-1,8(2H,5H,9H,10H)-dione
    Bueyuekguengoer, Orhan
    Kaya, Muharrem
    Odabasoglu, Mustafa
    Yildirir, Yilmaz
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2007, 63 : O2275 - O2277
  • [22] 10-(4-chlorophenyl)-9-(4-fluorophenyl)-3,3,6,6-tetramethyl-3,4,6,7,9,10-hexahydroacridine-1,8(2H,5H)-dione
    Zhao, Ling-Ling
    Teng, Da
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2008, 64 : O1772 - U2091
  • [23] 9-(2,4-Difluorophenyl)-3,3,6,6-tetramethyl-3,4,5,6,7,9-hexahydro-2H-xanthene-1,8-dione
    Begum, S. Rizwana
    Hema, R.
    Sumathi, G.
    Valliappan, R.
    Srinivasan, N.
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2014, 70 : O276 - +
  • [24] 3,3,6,6-Tetramethyl-9-(2-nitrophenyl)-3,4,6,7-tetrahydro-2H-xanthene-1,8(5H,9H)-dione
    Mo, Yingming
    Zang, Hong-Jun
    Cheng, Bo-Wen
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2010, 66 : O2129 - U2168
  • [25] Synthesis and characterization of 9-(4-nitrophenyl)3,3,6,6-tetramethyl-3,4,6,7,9,10-hexahydro-1,8(2H,5H) acridinedione and its methoxyphenyl derivative
    K. Palani
    D. Thirumalai
    P. Ambalavanan
    M. N. Ponnuswamy
    V. T. Ramakrishnan
    Journal of Chemical Crystallography, 2005, 35 : 751 - 760
  • [26] Crystal structure, Hirshfeld surface and frontier molecular orbital analysis of 10-benzyl-9-(4-hydroxy-3-methoxyphenyl)-3,3,6,6-tetramethyl-3,4,6,7,9,10-hexahydroacridine-1,8(2H,5H)-dione
    Sughanya, V
    Loganathan, B.
    Praveenkumar, D.
    Ayyappan, J.
    Sundararajan, M. L.
    Prabhakaran, A.
    Dhandapani, A.
    Babu, N. Suresh
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2022, 78 : 789 - +
  • [27] Synthesis and characterization of 9-(4-nitrophenyl)3,3,6,6-tetramethyl-3,4,6,7,9,10-hexahydro-1,8(2H,5H) acridinedione and its methoxyphenyl derivative
    Palani, K
    Thirumalai, D
    Ambalavanan, P
    Ponnuswamy, MN
    Ramakrishnan, VT
    JOURNAL OF CHEMICAL CRYSTALLOGRAPHY, 2005, 35 (10) : 751 - 760
  • [28] 3,3,6,6-Tetramethyl-9-(2-nitrophenyl)-3,4,5,6,9,10-hexahydroacridin e-1,8(2H,7H)-dione
    Unidad Profesional, Interdisciplinaria de, Biotecnologia-IPN, Mexico DF, Mexico
    Acta Crystallogr Sect C Cryst Struct Commun, pt 11 (2811-2814):
  • [29] 10-Amino-3,3,6,6-tetramethyl-9-(4-bromophenyl)-3,4,5,6,9,10-hexahydroacridine-1,8(2H,7H)-dione
    Tu, SJ
    Zhang, JP
    Zhu, XT
    Xu, JN
    Wang, Q
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2005, 61 : O1491 - O1493
  • [30] 4a-Hydroxy-9-(4-hydroxyphenyl)-4,4a,5,6,9,9a-hexahydro-3H-xanthene-1,8(2H,7H)-dione
    Wang, Liying
    Lu, Weicheng
    Yang, Yan
    Zhu, Yulin
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2011, 67 : O2751 - +