Flow-injection determination of ornidazole by chemiluminescence detection based on a luminol-ferricyanide reaction

被引:14
|
作者
Lv, Y [1 ]
Zhang, ZJ [1 ]
He, DY [1 ]
Hu, YF [1 ]
机构
[1] SW Normal Univ, Dept Chem, Inst Analyt Sci, Chongqing 400715, Peoples R China
关键词
D O I
10.2116/analsci.19.625
中图分类号
O65 [分析化学];
学科分类号
070302 ; 081704 ;
摘要
A flow-injection analysis (FIA) with a chemiluminescence detection method was developed for the determination of ornidazole based on the inhibition intensity of chemiluminescence from the luminol-ferricyanide system. Under the condition of 1.0 x 10(-3) mol/L luminol and 5.0 x 10(-6) mol/L potassium ferricyanide, the response to the concentration of ornidazole is linear from 0.2 mug ml(-1) to 10 mug ml(-1), and a detection limit of 0.05 mug ml(-1) can be obtained. This method has been successfully applied to the determination of ornidazole in pharmaceutical preparations.
引用
收藏
页码:625 / 627
页数:3
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