Synthesis and characterization of biosynthetic polymers based on (2E)-3-(4-hydroxy-3-methoxy)-2-phenylpropenoic acid

被引:1
|
作者
Karmanov, A. P. [1 ,2 ]
Derkacheva, O. Yu. [3 ]
Kocheva, L. S. [2 ,4 ]
机构
[1] Russian Acad Sci, Komi Sci Ctr, Inst Biol, Ural Branch, 28 Ul Kommunisticheskaya, Syktyvkar 167982, Russia
[2] Pitirim Sorokin Syktyvkar State Univ, 55 Oktyabrskii Prosp, Syktyvkar 167001, Russia
[3] St Petersburg State Univ Ind Technol & Design, Higher Sch Technol & Energet, 4 Ul Ivana Chernykh, St Petersburg 198095, Russia
[4] Russian Acad Sci, Ural Branch, Komi Sci Ctr, Inst Geol, 54 Ul Pervomaiskaya, Syktyvkar 167982, Russia
关键词
ferulic acid; biosynthetic polymers; IR spectroscopy; C-13 NMR spectroscopy; chemical structure; topological structure of macromolecules; FERULIC ACID; FTIR-SPECTROSCOPY; LIGNIN;
D O I
10.1007/s11172-018-2144-1
中图分类号
O6 [化学];
学科分类号
0703 ;
摘要
The polymers obtained by the dehydrogenization enzymatic polymerization of (2E)-3-(4- hydroxy-3-methoxy)-2-phenylpropenoic acid (ferulic acid) in the peroxidase-hydrogen peroxide system were studied by D-13<inverted exclamation> NMR and FTIR spectroscopy, elemental analysis, sedimentation diff usion analysis, and viscometry. The amount of the main structure fragments of the macromolecules was established, and comparative analysis of the chemical structures of the polymers was carried out. Differences in the topological structures of macromolecules of the biosynthetic polymers based on ferulic acid were revealed.
引用
收藏
页码:826 / 832
页数:7
相关论文
共 50 条
  • [21] (2E)-2-(3,5-dimethoxyphenyl)-3-(4-ethoxy-3-iodo-phenyl)acrylic acid
    Chen, K
    Adelstein, SJ
    Kassis, AI
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2005, 61 : O3517 - O3519
  • [22] Study on the second-order nonlinear optical properties of 4-Hydroxy-3-Methoxy Cinnamylic Acid
    Zhao, B
    Qi, TL
    ACTA PHYSICA SINICA, 2001, 50 (09) : 1699 - 1702
  • [23] A Fluorescence study of Solubilization of 4-Hydroxy-3-Methoxy Benzoic Acid (4-H-3-MBA) in Surfactant Micelles
    Acharya, Seema
    Mahlawat, Anshu
    RESEARCH JOURNAL OF PHARMACEUTICAL BIOLOGICAL AND CHEMICAL SCIENCES, 2015, 6 (03): : 887 - 892
  • [24] Synthesis, characterization and conductivity study of poly(vinyl 4-hydroxy-3-methoxy benzal) and its sodio salt in solid state
    Borah, P
    Hussain, S
    Dutta, A
    SOLID STATE IONICS: THE SCIENCE AND TECHNOLOGY OF IONS IN MOTION, 2004, : 483 - 488
  • [25] Synthesis, spectroscopic characterization:: (IR, multinuclear NMR, 119mSn Mossbauer and mass spectrometry), and biological activity (antibacterial, antifungal, and cytotoxicity) of di- and triorganotin(IV) complexes of (E)-3-(4-chlorophenyl)-2-phenylpropenoic acid
    Sadiq-ur-Rehman
    Ali, S
    Badshah, A
    Mazhar, M
    Song, XQ
    Eng, G
    Khan, KM
    SYNTHESIS AND REACTIVITY IN INORGANIC AND METAL-ORGANIC CHEMISTRY, 2004, 34 (08): : 1379 - 1399
  • [26] Synthesis of 8-hydroxy-6-methoxy-3-undecylisocoumarin and 2-hydroxy-4-methoxy-6-(2-oxotridecyl)benzoic acid
    Saeed, A
    Iqbal, R
    Rama, NH
    JOURNAL OF THE CHEMICAL SOCIETY OF PAKISTAN, 1995, 17 (04): : 236 - 239
  • [27] (E)-3-[(2-Hydroxy-3-methoxybenzylidene) amino] benzoic acid
    Kargar, Hadi
    Sharafi, Zahra
    Kia, Reza
    Ghelenji, Safoora
    Tahir, Muhammad Nawaz
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2012, 68 : O1067 - +
  • [28] Encapsulation of 4-hydroxy-3-methoxy benzoic acid and 4-hydroxy-3,5-dimethoxy benzoic acid with native and modified cyclodextrins
    Rajendiran, N.
    Jenita, M. Jude
    SPECTROCHIMICA ACTA PART A-MOLECULAR AND BIOMOLECULAR SPECTROSCOPY, 2015, 136 : 1349 - 1357
  • [29] Single-crystal growth of 4-hydroxy-3-methoxy benzaldehyde by the Bridgman technique and its characterization
    Kannan, V.
    Jayaprakasan, M.
    Ganesh, R. Bairava
    Ramasamy, P.
    PHYSICA STATUS SOLIDI A-APPLICATIONS AND MATERIALS SCIENCE, 2006, 203 (10): : 2488 - 2495
  • [30] (E)-3-(2-Hydroxy-4-methoxybenzylideneamino)benzonitrile
    Zhou, Jian-Cheng
    Zhang, Zheng-Yun
    Zhang, Chuan-Ming
    Li, Nai-Xu
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2009, 65 : 01644 - U3029