Investigation of the free volume in olanzapine by PALS

被引:3
|
作者
Jasinska, B. [1 ]
Kedzior, M. [1 ]
Sniegocka, M. [2 ]
Koziol, A. E. [2 ]
Wawrzycka-Gorczyca, I. [2 ]
机构
[1] Marie Curie Sklodowska Univ, Inst Phys, Pl Marii Curie Sklodowskiej 1, PL-20031 Lublin, Poland
[2] Marie Curie Sklodowska Univ, Fac Chem, Pl Marii Curie Sklodowskiej 1, PL-20031 Lublin, Poland
关键词
LIFETIMES;
D O I
10.1002/pssc.200982110
中图分类号
T [工业技术];
学科分类号
08 ;
摘要
Two polymorphic forms of olanzapine were investigated as a function of temperature in a range from 100 to 420 K and as a function of hydrostatic pressure from 0 to 1300 MPa using positron annihilation lifetime spectroscopy. In the crystallographic structure of both investigated forms exists component ascribed to positronium formation. The lifetime value of o-Ps changes nonmonotinicaly from 1.0 to 1.6 ns as a function of temperature. (C) 2009 WILEY-VCH Verlag GmbH & Co. KGaA, Weinheim
引用
收藏
页码:2432 / +
页数:2
相关论文
共 50 条
  • [1] Investigation of free volume in epoxy resins studied by PALS
    Wang, Junjun
    Wang, Bo
    Zhou, Wei
    Gong, Jing
    Gong, Zhenli
    Yue, Shaojie
    POSITRON AND POSITRONIUM CHEMISTRY, 2009, 607 : 82 - 84
  • [2] Investigation of Free Volume Size and Mechanical Properties for PolymethylMethacrylate/Organic Rectorite Composites by PALS
    Zhou, Wei
    Gong, Yansheng
    FUNDAMENTAL OF CHEMICAL ENGINEERING, PTS 1-3, 2011, 233-235 : 1868 - 1871
  • [3] Interfacial free volume measurements of epoxy on aluminum by PALS
    Madani, MM
    Miron, RR
    Granata, RD
    ANTEC '99: PLASTICS BRIDGING THE MILLENNIA, CONFERENCE PROCEEDINGS, VOLS I-III: VOL I: PROCESSING; VOL II: MATERIALS; VOL III: SPECIAL AREAS;, 1999, : 2202 - 2206
  • [4] Microstructure of free volume in SMA copolymers II. Local free volume from PALS
    Kilburn, D
    Dlubek, G
    Pionteck, J
    Bamford, D
    Alam, MA
    POLYMER, 2005, 46 (03) : 869 - 876
  • [5] Free volume from PALS and atomistic simulations: The OTP case
    Bartos, J
    Urban, J
    Mach, P
    Kristiak, J
    POSITRON ANNIHILATION - ICPA-12, 2001, 363-3 : 294 - 296
  • [6] Study on damping mechanism based on the free volume for CIIR by PALS
    Zhu, Yuchan
    Zhou, Wei
    Wang, Junjun
    Wang, Bo
    Wu, Jinrong
    Huang, Guangsu
    JOURNAL OF PHYSICAL CHEMISTRY B, 2007, 111 (39): : 11388 - 11392
  • [7] PALS free volume study of dry and water saturated epoxies
    Madani, MM
    Miron, RR
    Granata, RD
    JOURNAL OF COATINGS TECHNOLOGY, 1997, 69 (872): : 45 - &
  • [8] Encapsulation of natural flavors in cyclodextrins: free volume studies by PALS
    Ferreira Marques, M. F.
    Gordo, P. M.
    Santos, S. D.
    Marques, R. F.
    Moreira da Silva, A.
    Kajcsos, Zs
    POSITRON AND POSITRONIUM CHEMISTRY X, 2013, 733 : 88 - 91
  • [9] PALS free volume and mechanical properties in dimethacrylate-based thermosets
    Rey, L
    Galy, J
    Sautereau, H
    Simon, GP
    Cook, WD
    POLYMER INTERNATIONAL, 2004, 53 (05) : 557 - 568
  • [10] Comparison of the free volume sizes and shapes determined from crystallographic and PALS data
    Tydda, Maciej
    Jasinska, Bozena
    NUKLEONIKA, 2015, 60 (04) : 771 - 775