The synthesis of quinoxalines by condensation reaction of acyloins with o-phenylenediamine without solvent under microwave irradiation

被引:0
|
作者
Feng, JC [1 ]
Liu, Y [1 ]
Meng, QH [1 ]
Liu, B [1 ]
机构
[1] Nanjing Univ, Dept Chem, Nanjing 210093, Peoples R China
关键词
D O I
暂无
中图分类号
O62 [有机化学];
学科分类号
070303 ; 081704 ;
摘要
A convenient synthetic method for 2,3-disubstituted quinoxalines is described. Heating the aryl or alkyl acyloins and o-phenylenediamine in a microwave oven for 3-6 minutes affords 2,3-disubstituted quinoxalines in 20-94% yields.
引用
收藏
页码:193 / 196
页数:4
相关论文
共 50 条
  • [21] Investigation on the Reaction Mechanism for the Synthesis of Benzimidazole Derivatives from Aldehydes and o-Phenylenediamine
    Cui, Lijun
    Xiao, Shangyou
    Yang, Haoshu
    Xu, Pan
    Cheng, Fansheng
    Li, Zhenghua
    Liang, Ronghui
    Xia, Zhining
    CHINESE JOURNAL OF ORGANIC CHEMISTRY, 2011, 31 (05) : 672 - 676
  • [22] Synthesis of aromatic ethers without organic solvent and inorganic carrier under microwave irradiation
    Wang, JX
    Zhang, ML
    Xing, ZL
    Hu, YL
    SYNTHETIC COMMUNICATIONS, 1996, 26 (02) : 301 - 305
  • [23] Manganese(IV) dioxide-catalyzed synthesis of quinoxalines under microwave irradiation
    Kim, SY
    Park, KH
    Chung, YK
    CHEMICAL COMMUNICATIONS, 2005, (10) : 1321 - 1323
  • [24] Solvent-free Knoevenagel condensation reaction under microwave irradiation exploiting a new reagent: antimony trichloride
    Mitra, AK
    Karchaudhuri, N
    De, A
    JOURNAL OF THE INDIAN CHEMICAL SOCIETY, 2005, 82 (02) : 177 - 179
  • [25] Solvent free synthesis of quinoxalines, dipyridophenazines and chalcones under microwave irradiation with sulfated Degussa titania as a novel solid acid catalyst
    Krishnakumar, B.
    Swaminathan, M.
    JOURNAL OF MOLECULAR CATALYSIS A-CHEMICAL, 2011, 350 (1-2) : 16 - 25
  • [26] Coumarins: Fast synthesis by Knoevenagel condensation under microwave irradiation
    Bogdal, D
    JOURNAL OF CHEMICAL RESEARCH-S, 1998, (08): : 468 - 469
  • [27] Ecofriendly fast batch synthesis of dioxolanes, dithiolanes, and oxathiolanes without solvent under microwave irradiation
    Perio, B
    Dozias, MJ
    Hamelin, J
    ORGANIC PROCESS RESEARCH & DEVELOPMENT, 1998, 2 (06) : 428 - 430
  • [28] Efficient synthesis of new nitrogen donor containing tripods under microwave irradiation and without solvent
    Touzani, R
    Ramdani, A
    Ben-Hadda, T
    El Kadiri, S
    Maury, O
    Le Bozec, H
    Dixneuf, PH
    SYNTHETIC COMMUNICATIONS, 2001, 31 (09) : 1315 - 1321
  • [29] Fast synthesis of aromatic aldehydes from benzylic bromides without solvent under microwave irradiation
    Barbry, D
    Champagne, P
    TETRAHEDRON LETTERS, 1996, 37 (43) : 7725 - 7726
  • [30] FAST SYNTHESIS OF AMINO-ACID SALTS AND LACTAMS WITHOUT SOLVENT UNDER MICROWAVE IRRADIATION
    LAURENT, A
    JACQUAULT, P
    DIMARTINO, JL
    HAMELIN, J
    JOURNAL OF THE CHEMICAL SOCIETY-CHEMICAL COMMUNICATIONS, 1995, (11) : 1101 - 1101