Synthesis and crystal structure of N-[4-(4-methyl-phenylsulfamoyl)-phenyl]4-methyl-1,2,3-thiadiazole-5-carboxamide

被引：0
|
作者：
Wang Jian-Guo [1 ]
Xiao Yong-Jun [1 ]
Li Zheng-Ming [1 ]
Song Hai-Bin [1 ]
机构：
[1] Nankai Univ, Inst Elementoorgan Chem, State Key Lab Elementoorgan Chem, Tianjin 300071, Peoples R China
来源：
CHINESE JOURNAL OF STRUCTURAL CHEMISTRY | 2007年 / 26卷 / 05期
关键词：
X-ray diffraction; crystal structure; synthesis;
D O I：
暂无
中图分类号：
O61 [无机化学];
学科分类号：
070301 ; 081704 ;
摘要：
The crystal structure of the title compound (C17H16N4O3S2, M-r= 388.46) has been determined by single-crystal X-ray diffraction. The crystal belongs to monoclinic, space group P2(1)/c with a=13.688(2), h = 16.704(3), c = 8.3308(12) angstrom, beta = 99.474(6)degrees, V = 1878.8(5) A(3), M-r. = 388.46, Z = 4, D-c = 1.373 g/cm(3), mu = 0.308 mm(-1), F(000) = 808, R = 0.0389 and wR = 0.0917. X-ray analysis reveals that the crystal structure involves intermolecular N-H...O and N-H...N hydrogen bonds, which link the molecules into a layer parallel to the ac plane.
引用
收藏
页码：501 / 504
页数：4
相关论文
共 50 条
  • [31] Synthesis, Crystal Structure and Anti-TMV Activity of(Z)-4-[3-(4-Methyl-1,2,3-thiadiazol-5-yl)-3-(4-trifluoromethylphenyl)acryloyl]morpholine
    孙素素
    李晴
    高卫
    李晓天
    陈来
    张金林
    Chinese Journal of Structural Chemistry, 2021, 40 (01) : 109 - 113
  • [32] METHYLATION OF 4-PHENYL-1,2,3-THIADIAZOLE - REACTION OF NUCLEOPHILES WITH N-METHYL-1,2,3-THIADIAZOLIUM SALTS AND THE CRYSTAL-STRUCTURE OF THE PRODUCTS
    AURICCHIO, S
    BRUCKNER, S
    MALPEZZIGIUNCHI, L
    KOZINSKY, VA
    ZELENSKAJA, OV
    JOURNAL OF HETEROCYCLIC CHEMISTRY, 1980, 17 (06) : 1217 - 1219
  • [33] Reactivity ratios of N-[4-(aminosulfonyl) phenyl] acrylamide/acrylonitrile and N-[4-(aminosulfonyl) phenyl] acrylamide/methyl methacrylate copolymerization systems
    Gao, YX
    Bao, YZ
    Huang, ZM
    Weng, ZX
    ACTA POLYMERICA SINICA, 2004, (03) : 450 - 453
  • [34] Synthesis, Crystal Structure, and Spectroscopic and Electronic Properties of N-[4-(3-Methyl-3-Phenyl-Cyclobutyl)-Thiazol-2-yl]-N′-Phenyl Hydrazine
    Saracoglu, H.
    Guntepe, F.
    Yuksektepe, C.
    Caliskan, N.
    Cukurovali, A.
    MOLECULAR CRYSTALS AND LIQUID CRYSTALS, 2011, 548 : 237 - 255
  • [35] 5-Methyl-N-[2-(trifluoromethyl)phenyl]isoxazole-4-carboxamide
    Wang, De-Cai
    Qiu, Jiang-Kai
    Zhu, Hai-Xi
    Wei, Ping
    Ou-Yang, Ping-Kai
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2012, 68 : O1450 - +
  • [36] Synthesis and crystal structure of N-(1-phenyl-3-methyl-4-benzylidene-5-pyrazolone) p-nitrobenzoylhydrazide
    Ji, YL
    Liu, L
    Jia, DZ
    Yu, KB
    CHINESE JOURNAL OF STRUCTURAL CHEMISTRY, 2002, 21 (05) : 553 - 556
  • [37] Crystal structure of 4-methyl-1,2,4-triazole-thione
    El Hajji, A
    El Ammari, L
    Mattern, G
    Benarafa, L
    Idrissi, MS
    JOURNAL DE CHIMIE PHYSIQUE ET DE PHYSICO-CHIMIE BIOLOGIQUE, 1998, 95 (09) : 2102 - 2108
  • [38] Synthesis and crystal structure of 2-benzoyl-4-methyl phenyl benzoate
    Mahendra, M
    Doreswamy, BH
    Sridhar, MA
    Prasad, JS
    Khanum, SA
    Shashikanth, S
    Venu, TD
    JOURNAL OF CHEMICAL CRYSTALLOGRAPHY, 2005, 35 (06) : 463 - 467
  • [39] Synthesis and crystal structure of 2-benzoyl-4-methyl phenyl benzoate
    M. Mahendra
    B. H. Doreswamy
    M. A. Sridhar
    J. Shashidhara Prasad
    S. A. Khanum
    S. Shashikanth
    T. D. Venu
    Journal of Chemical Crystallography, 2005, 35 : 463 - 467
  • [40] Novel Derivatives of 4-Methyl-1,2,3-Thiadiazole-5-Carboxylic Acid Hydrazide: Synthesis, Lipophilicity, and In Vitro Antimicrobial Activity Screening
    Paruch, Kinga
    Popiolek, Lukasz
    Biernasiuk, Anna
    Berecka-Rycerz, Anna
    Malm, Anna
    Gumieniczek, Anna
    Wujec, Monika
    APPLIED SCIENCES-BASEL, 2021, 11 (03): : 1 - 12
12345