Reaction of rhodium trichloride with oxyethylated calix[4]resorcinarene

被引：0

作者：

Guseva, E. V. ^{[1
]}

Kasymova, E. M. ^{[2
]}

Egorov, G. V. ^{[1
]}

Kayupov, A. R. ^{[2
]}

Khamatgalimov, A. R. ^{[2
]}

Khasanshin, R. A. ^{[3
]}

Burilov, A. R. ^{[2
]}

机构：

[1] Kazan State Technol Univ, Kazan 420015, Tatarstan, Russia

[2] Russian Acad Sci, Kazan Res Ctr, AE Arbuzov Organ & Phys Chem Inst, Kazan 420088, Tatarstan, Russia

[3] Kazanorgsintez Co, Kazan 420015, Tatarstan, Russia

来源：

RUSSIAN JOURNAL OF GENERAL CHEMISTRY | 2010年 / 80卷 / 03期

基金：

俄罗斯基础研究基金会;

关键词：

VIBRATIONAL-SPECTRA; PLATINUM METALS; COMPLEXES;

D O I：

10.1134/S1070363210030199

中图分类号：

O6 [化学];

学科分类号：

0703 ;

摘要：

Reaction of rhodium trichloride with a new ligand, oxyethylated calix[4]resorcinarene was examined in an inert atmosphere in different solvents (acetone, acetone + chloroform). The product was characterized by IR, Raman, H-1 NMR, ESR, ESCA spectroscopy, conductometry. Its composition was proved by the data of elemental and X-ray fluorescent analyses. The solvent used does not affect the composition of the product but only its yield. The structure of the coordination node and the type of coordination of the rhodium-containing fragment was investigated by calculating the model molecules of the ligand and the complex using the molecular mechanics method (MM+).

引用

页码：478 / 484

页数：7

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