Influence of the H2O content and the time on the formation of nanostructures in a chemical solution of H2O/HF/NH4F/EG

被引:1
|
作者
Bautista-Ruiz, J. H. [1 ]
Raba, A. M. [1 ]
Joya, M. R. [2 ]
机构
[1] Univ Francisco de Paula Santander, Dept Fis, San Jose De Cucuta, Colombia
[2] Univ Nacl Colombia, Dept Fis, Bogota, Colombia
关键词
NANOTUBES; TITANIUM;
D O I
10.1088/1742-6596/1126/1/012042
中图分类号
T [工业技术];
学科分类号
08 ;
摘要
The influence of anodizing time on the length, morphology and photoelectrochemical properties of TiO2 Nanotubes has been investigated. An optimum anodizing time of 20 min at 20V leads to 220nm long of the nanotubes. By having a detailed control of the electric current one can know exactly the time in which the nanotubes grew and the time in which the process stopped. The FEG-SEM measures show the morphology of the nanotubes and how they come to separate and fall after a certain time. However, the growth of these, is uniform with little remaining material on the surface. For the solution of the anodizing process it is very important to control the amount of water, ethylene glycol and hydrofluoric acid. Small modifications in the solution change the growth time and size of the nanotubes.
引用
收藏
页数:4
相关论文
共 50 条
  • [41] Excess electron binding by (H2O)2, (H2O)3, H2O...NH3, and H2O...HCl.
    Gutowski, MS
    Skurski, P
    ABSTRACTS OF PAPERS OF THE AMERICAN CHEMICAL SOCIETY, 1999, 218 : U357 - U357
  • [42] SYNTHESES OF NA[V(EDTA)(H2O)].NH2O, K[V(EDTA)(H2O)].NH2O, NH4[V(EDTA)(H2O)].NH2O AND X-RAY CRYSTAL-STRUCTURE OF NA[V(EDTA)(H2O)].3H2O
    SHIMOI, M
    SAITO, Y
    OGINO, H
    CHEMISTRY LETTERS, 1989, (09) : 1675 - 1678
  • [43] ONE-ELECTRON ENERGY LEVELS IN CU(H2O)4TIF6,NH4F
    PALMER, RA
    ROY, CG
    ROY, RC
    JOURNAL OF THE CHEMICAL SOCIETY A -INORGANIC PHYSICAL THEORETICAL, 1971, (19): : 3084 - &
  • [44] Synthesis and crystal structure of [Zn(H2O)4(C4H2O4)] • H2O
    XIe, HZ
    Zheng, YQ
    Shou, KQ
    JOURNAL OF COORDINATION CHEMISTRY, 2003, 56 (15) : 1291 - 1297
  • [45] Crystal structures of [Mn2(H2O)4(phen)2(C4H4O4)2] • 2 H2O and [Mn(phen)2(H2O)2][Mn(phen)2(C4H4O4)](C4H4O4) •7 H2O
    Zheng, YQ
    Lin, JL
    Sun, J
    ZEITSCHRIFT FUR ANORGANISCHE UND ALLGEMEINE CHEMIE, 2001, 627 (05): : 1059 - 1065
  • [46] Double Photodetachment of F-•H2O: Experimental and Theoretical Studies of [F•H2O]+
    Shahi, Abhishek
    McCaslin, Laura
    Albeck, Yishai
    Continetti, Robert E.
    Gerber, R. Benny
    Strasser, Daniel
    JOURNAL OF PHYSICAL CHEMISTRY LETTERS, 2018, 9 (23): : 6808 - 6813
  • [47] Hydration of zinc ions:: theoretical study of [Zn(H2O)4](H2O)82+ and [Zn(H2O)6](H2O)62+
    Díaz, N
    Suárez, D
    Merz, KM
    CHEMICAL PHYSICS LETTERS, 2000, 326 (3-4) : 288 - 292
  • [48] THE INFLUENCE OF H2O DEFORMATION ON A DEVIATION ON O-H CHEMICAL BOND
    Yushko, O. O.
    Okhrimenko, B. A.
    UKRAINIAN JOURNAL OF PHYSICS, 2012, 57 (02): : 278 - 282
  • [49] GaSb AND GaAs CHEMICAL POLISHING BY HF:H2O2:CITRIC ACID: H2O
    Rosendo, E. R.
    Olvera, J. O.
    Diaz, T. D.
    Rojas, M. R.
    de Anda, F.
    ACTA CRYSTALLOGRAPHICA A-FOUNDATION AND ADVANCES, 2002, 58 : C162 - C162
  • [50] Chemical Effect of H2O on CH4 Oxidation during Combustion in O2/H2O Environments
    Hong, Dikun
    Liu, Liang
    Huang, Yu
    Zheng, Chuguang
    Guo, Xin
    ENERGY & FUELS, 2016, 30 (10) : 8491 - 8498