Mechanochemical synthesis of vanadium nitride

被引：49
|
作者：
Roldan, M. A. [1 ]
Lopez-Flores, V. [1 ]
Alcala, M. D. [1 ]
Ortega, A. [1 ]
Real, C. [1 ]
机构：
[1] Ctr Mixto CSIC UNSE, Inst Ciencia Mat, Seville 41092, Spain
来源：
JOURNAL OF THE EUROPEAN CERAMIC SOCIETY | 2010年 / 30卷 / 10期
关键词：
Mechanosynthesis; Vanadium nitride; EELS; XAS; Microhardness; NANOCRYSTALLINE VN; SUPERCONDUCTING PROPERTIES; CARBOTHERMAL SYNTHESIS; CATALYSTS; REDUCTION; POWDERS; DEPOSITION; DILUTION; CARBIDES; SYSTEMS;
D O I：
10.1016/j.jeurceramsoc.2010.04.008
中图分类号：
TQ174 [陶瓷工业]; TB3 [工程材料学];
学科分类号：
0805 ; 080502 ;
摘要：
Vanadium nitride (VN) has been prepared by mechanosynthesis from vanadium metal under a pressurized nitrogen atmosphere in a short milling time. The characterization of the final product by X-ray diffraction, scanning electron microscopy, electron energy loss (EELS), and X-ray absorption spectroscopy (XAS) is presented. The final product, VN with 96% of purity, is obtained at room temperature with nanometric particle size and a very high microhardness after sintering. A relationship between microstructure and microhardness as well as a comparison between the VN obtained mechanical and thermal method is also presented. (c) 2010 Elsevier Ltd. All rights reserved.
引用
收藏
页码：2099 / 2107
页数：9
相关论文
共 50 条
  • [21] Synthesis of tungsten, molybdenum and vanadium bronzes by mechanochemical method milling with liquid hydrocarbons
    Takai, S
    Hoshimi, N
    Esaka, T
    ELECTROCHEMISTRY, 2004, 72 (12) : 876 - 879
  • [22] Synthesis and microwave absorption properties of porous vanadium nitride microspheres
    Runkang Li
    Chaojie Li
    Fan Zhang
    Yi Cui
    Dongfeng LV
    Yuejun Chen
    Yingna Wei
    Hengyong Wei
    Jinglong Bu
    Journal of Materials Science: Materials in Electronics, 2022, 33 : 17306 - 17321
  • [23] SYNTHESIS OF VANADIUM NITRIDE IN AN ULTRAHIGH-FREQUENCY DISCHARGE PLASMA
    TROITSKII, VN
    GREBTSOV, BM
    ALEKSEEV, NV
    HIGH ENERGY CHEMISTRY, 1976, 10 (01) : 69 - 71
  • [24] Synthesis and microwave absorption properties of porous vanadium nitride microspheres
    Li, Runkang
    Li, Chaojie
    Zhang, Fan
    Cui, Yi
    Lv, Dongfeng
    Chen, Yuejun
    Wei, Yingna
    Wei, Hengyong
    Bu, Jinglong
    JOURNAL OF MATERIALS SCIENCE-MATERIALS IN ELECTRONICS, 2022, 33 (21) : 17306 - 17321
  • [25] Kinetics and mechanism of mechanochemical synthesis of hafnium nitride ceramics in a planetary ball mill
    Nepapushev, A. A.
    Buinevich, V. S.
    Gallington, L. C.
    Pauls, J. M.
    Orlova, T.
    Miloserdova, O. M.
    Chapysheva, N. V.
    Rogachev, A. S.
    Mukasyan, A. S.
    CERAMICS INTERNATIONAL, 2019, 45 (18) : 24818 - 24826
  • [26] Mechanochemical synthesis of graphitic carbon nitride/graphene oxide nanocomposites for dye sorption
    Molla, Aniruddha
    Youk, Ji Ho
    DYES AND PIGMENTS, 2023, 220
  • [27] Rapid mechanochemical synthesis of nickel-vanadium carbide nanocomposite powder by magnesiothermic reaction
    Davoodi, Danial
    Emami, Amir Hossein
    Tayebi, Morteza
    Hosseini, Seyed Kamal
    CERAMICS INTERNATIONAL, 2018, 44 (05) : 5411 - 5419
  • [28] In situ synthesis of vanadium carbide-copper nanocomposite by a modified mechanochemical combustion method
    Hassanzadeh-Tabrizi, S. A.
    Badr, Homa Hosseini
    Alizadeh, Sara
    CERAMICS INTERNATIONAL, 2016, 42 (08) : 9371 - 9374
  • [29] MECHANOCHEMICAL POLISHING OF SILICON-NITRIDE
    VORA, H
    ORENT, TW
    STOKES, RJ
    JOURNAL OF THE AMERICAN CERAMIC SOCIETY, 1982, 65 (09) : C140 - C141
  • [30] Compton profile of vanadium carbide and vanadium nitride
    Deb, A
    Chatterjee, AK
    PHYSICAL REVIEW B, 1996, 53 (20): : 13393 - 13399
12345