Oxidation of 3,4-dihydropyrimidin-2(1H)-ones with nitrosonium (NO+)

被引：10

作者：

Liang, Rui Rui ^{[1
]}

Wu, Guai Li ^{[1
]}

Wu, Wen Tao ^{[1
]}

Wu, Long Min ^{[1
]}

机构：

[1] Lanzhou Univ, State Key Lab Appl Organ Chem, Lanzhou 730000, Peoples R China

来源：

CHINESE CHEMICAL LETTERS | 2009年 / 20卷 / 10期

基金：

中国国家自然科学基金;

关键词：

Dihydropyrimidinone; Nitrosonium; Oxidation; PHENYL 2,4,6-TRINITROPHENYL ETHER; AROMATIC-SUBSTITUTION REACTIONS; NONPOLAR APROTIC-SOLVENT; SOLID-PHASE SYNTHESIS; NITRIC-OXIDE; HANTZSCH 1,4-DIHYDROPYRIDINES; ELECTROCHEMICAL OXIDATION; PYRIMIDINE; BIGINELLI; DIHYDROPYRIMIDINONES;

D O I：

10.1016/j.cclet.2009.04.039

中图分类号：

O6 [化学];

学科分类号：

0703 ;

摘要：

3, 4-Dihydropyrimidin-2(1H)-ones (DHPMs) were oxidized with 1.2 equiv. of nitrosonium tetrafluoroborate (NO+BF4-) to pyrimidin-2(1H)-ones in acetonitrile at room temperature in high yields. (C) 2009 Long Min Wu. Published by Elsevier B.V. on behalf of Chinese Chemical Society. All rights reserved.

引用

页码：1183 / 1186

页数：4

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