Krohnke reaction in aqueous media:: one-pot clean synthesis of 4′-aryl-2,2′:6′,2"-terpyridines

被引：107
|
作者：
Tu, Shujiang [1 ]
Jia, Runhong
Jiang, Bo
Zhang, Junyong
Zhang, Yan
Yao, Changsheng
Ji, Shunjun
机构：
[1] Xuzhou Normal Univ, Dept Chem, Xuzhou 221116, Jiangsu, Peoples R China
[2] Suzhou Univ, Coll Chem & Chem Engn, Key Lab Organ Synth Jiangsu Prov, Suzhou 215006, Peoples R China
来源：
TETRAHEDRON | 2007年 / 63卷 / 02期
基金：
中国国家自然科学基金;
关键词：
D O I：
10.1016/j.tet.2006.10.069
中图分类号：
O62 [有机化学];
学科分类号：
070303 ; 081704 ;
摘要：
A clean aqueous Krohnke reaction process has been accomplished via a one-pot procedure of 2-acetylpyridine with aromatic aldehyde and ammonium acetate under microwave irradiation or conventional heating conditions. This method is convenient, economic and environmental friendly. (c) 2006 Elsevier Ltd. All rights reserved.
引用
收藏
页码：381 / 388
页数：8
相关论文
共 50 条
  • [41] CLEAN AND CONVENIENT ONE-POT SYNTHESIS OF 4-HYDROXYCOUMARIN AND 4-HYDROXY-2-QUINOLINONE DERIVATIVES
    Gao, Wen-Tao
    Hou, Wen-Duan
    Zheng, Mei-Ru
    Tang, Li-Jun
    SYNTHETIC COMMUNICATIONS, 2010, 40 (05) : 732 - 738
  • [42] An electrochemical tandem reaction: one-pot synthesis of homoallylic alcohols from alcohols in aqueous media
    Zhang, Li
    Zha, Zhenggen
    Zhang, Zhenlei
    Li, Yunfeng
    Wang, Zhiyong
    CHEMICAL COMMUNICATIONS, 2010, 46 (38) : 7196 - 7198
  • [43] A clean one-pot synthesis of tetrahydrobenzo[b]pyran derivatives catalyzed by hexadecyltrimethyl ammonium bromide in aqueous media
    Jin, TS
    Wang, AQ
    Wang, X
    Zhang, JS
    Li, TS
    SYNLETT, 2004, (05) : 871 - 873
  • [44] One-pot synthesis and evaluation of novel 3-aryl-6-ethoxycarbonyl-4-hydroxy-2H-pyran-2-one as a potent cytotoxic agent
    Dhage, Ganesh Raosaheb
    Thopate, Shankar Ramchandra
    Ramteke, Shefali Nishikant
    Kulkarni, Prasad Padmakar
    RSC ADVANCES, 2014, 4 (100): : 56870 - 56875
  • [45] ONE-POT SYNTHESIS OF 2-SPIROTHIAZOLIDIN-4-ONE DERIVATIVES
    ELZOHRY, MF
    ORGANIC PREPARATIONS AND PROCEDURES INTERNATIONAL, 1992, 24 (01) : 81 - 83
  • [46] Facile one-pot synthesis of 2-aryl-substituted nitriles and 2-aryl-3-keto nitriles via benzyne reaction
    Kamila, Sukanta
    Koh, Benjamin
    Biehl, Edward R.
    SYNTHETIC COMMUNICATIONS, 2006, 36 (23) : 3493 - 3507
  • [47] Synthesis of 1′-aryl-2′-(2-oxoindolin-3-yl)spiro[indoline-3,5′-pyrroline]-2,3′-dione via one-pot reaction of arylamines, acetone, and isatins
    Sun, Yan
    Sun, Jing
    Yan, Chao-Guo
    TETRAHEDRON LETTERS, 2012, 53 (28) : 3647 - 3649
  • [48] One-pot synthetic procedure for 2,2′-disubstituted biaryls via the Suzuki coupling reaction of aryl triflates in a biphasic solvent system
    Miura, Masanori
    Koike, Takanori
    Ishihara, Tsukasa
    Hirayama, Fukushi
    Sakamoto, Shuichi
    Okada, Minoru
    Ohta, Mitsuaki
    Tsukamoto, Shin-ichi
    SYNTHETIC COMMUNICATIONS, 2006, 36 (24) : 3809 - 3820
  • [49] One-pot chemoenzymatic synthesis of chiral disubstituted 1,2,3-triazoles in aqueous media
    de Oliveira, Camila de Souza
    de Andrade, Kleber Tellini
    Omori, Alvaro Takeo
    JOURNAL OF MOLECULAR CATALYSIS B-ENZYMATIC, 2013, 91 : 93 - 97
  • [50] 2,2′:6′,2"-Terpyridines Functionalized with Thienyl Substituents: Synthesis and Applications
    Husson, Jerome
    Knorr, Michael
    JOURNAL OF HETEROCYCLIC CHEMISTRY, 2012, 49 (03) : 453 - 478
12345