Krohnke reaction in aqueous media:: one-pot clean synthesis of 4′-aryl-2,2′:6′,2"-terpyridines

被引:107
|
作者
Tu, Shujiang [1 ]
Jia, Runhong
Jiang, Bo
Zhang, Junyong
Zhang, Yan
Yao, Changsheng
Ji, Shunjun
机构
[1] Xuzhou Normal Univ, Dept Chem, Xuzhou 221116, Jiangsu, Peoples R China
[2] Suzhou Univ, Coll Chem & Chem Engn, Key Lab Organ Synth Jiangsu Prov, Suzhou 215006, Peoples R China
基金
中国国家自然科学基金;
关键词
D O I
10.1016/j.tet.2006.10.069
中图分类号
O62 [有机化学];
学科分类号
070303 ; 081704 ;
摘要
A clean aqueous Krohnke reaction process has been accomplished via a one-pot procedure of 2-acetylpyridine with aromatic aldehyde and ammonium acetate under microwave irradiation or conventional heating conditions. This method is convenient, economic and environmental friendly. (c) 2006 Elsevier Ltd. All rights reserved.
引用
收藏
页码:381 / 388
页数:8
相关论文
共 50 条
  • [1] A convenient one-pot synthesis of 4′-aryl-2,2′:6′,2"-terpyridines and 2,4,6-triarylpyridines under microwave irradiation
    Tu, SJ
    Li, TJ
    Shi, F
    Wang, Q
    Zhang, JP
    Xu, JN
    Zhu, XT
    Zhang, XJ
    Zhu, SL
    Shi, DQ
    SYNTHESIS-STUTTGART, 2005, (18): : 3045 - 3050
  • [2] A facile route to sterically hindered and non-hindered 4′-aryl-2,2′:6′,2"-terpyridines
    Wang, JH
    Hanan, GS
    SYNLETT, 2005, (08) : 1251 - 1254
  • [3] Clean, one-pot synthesis of naphthopyran derivatives in aqueous media
    Jin, Tong-Shou
    Zhang, Jian-She
    Liu, Li-Bin
    Wang, Ai-Qing
    Li, Tong-Shuang
    SYNTHETIC COMMUNICATIONS, 2006, 36 (14) : 2009 - 2015
  • [4] Synthesis of 4′-substituted 2,2′:6′,2"-terpyridines via a Mitsunobu reaction
    Hovinen, J
    TETRAHEDRON LETTERS, 2004, 45 (29) : 5707 - 5709
  • [5] Convenient one-pot procedures for the synthesis of 2,2′:6′,2"-terpyridine
    Cooke, Michael W.
    Wang, Jianhua
    Theobald, Isabelle
    Hanan, Garry S.
    SYNTHETIC COMMUNICATIONS, 2006, 36 (12) : 1721 - 1726
  • [6] Green chemistry approach to the synthesis of 2-amino-4-aryl-6-ferrocenyl-pyridine derivatives by a one-pot reaction in aqueous medium
    Zhuang, Qiya
    Jia, Runhong
    Tu, Shujiang
    Zhang, Junyong
    Jiang, Bo
    Zhang, Yan
    JOURNAL OF HETEROCYCLIC CHEMISTRY, 2007, 44 (04) : 895 - 900
  • [7] Synthesis of 4′-substituted-2,2′:6′,2"-terpyridines
    Fallahpour, RA
    SYNTHESIS-STUTTGART, 2003, (02): : 155 - 184
  • [8] 4′-(4-fluorophenyl)-2,2′:6′,2"-terpyridine -: an aryl-2,2′:6′,2"-terpyridine with an electron-releasing aryl substituent
    Constable, EC
    Neuburger, M
    Smith, DR
    Zehnder, M
    INORGANICA CHIMICA ACTA, 1998, 276 (1-2) : 359 - 365
  • [9] One-Pot Synthesis of Substituted 2,2′-Bipyrroles. A Straightforward Route to Aryl Porphycenes
    Sanchez-Garcia, David
    Borrell, Jose I.
    Nonell, Santi
    ORGANIC LETTERS, 2009, 11 (01) : 77 - 79
  • [10] One-pot synthesis of 2-acylimino-3-aryl-1,3-thiazoline derivatives in aqueous media
    Wang, Xi Cun
    Wang, Fang
    Quan, Zheng Jun
    Zhang, Zhang
    Wang, Man Gang
    JOURNAL OF HETEROCYCLIC CHEMISTRY, 2006, 43 (06) : 1473 - 1477