A novel and convenient synthesis of 1,3,5-triazine-2,4(1H,3H)-diones

被引:7
|
作者
Shibuya, I [1 ]
Honda, K [1 ]
Gama, Y [1 ]
Shimizu, M [1 ]
机构
[1] Natl Inst Mat & Chem Res, Tsukuba, Ibaraki 3058565, Japan
关键词
silver cyanate; 5-aza uracil; N-substituted thiocarboamide;
D O I
10.3987/COM-99-8830
中图分类号
O62 [有机化学];
学科分类号
070303 ; 081704 ;
摘要
Several 1,3, 5-triazine-2,4(1H, 3H)-diones (1 - 5) were newly synthesized by the reaction of N-substituted thiocarboamides with silver cyanate. The structure was confirmed by the X-Ray structure analysis, and the pathway affording them was estimated.
引用
收藏
页码:929 / 933
页数:5
相关论文
共 50 条
  • [41] X-RAY STRUCTURE DETERMINATION AND NMR CHARACTERIZATION OF SOME FUSED HETEROCYCLES WITH A 1,3,5-TRIAZINE-2,4(1H,3H)-DIONE RING - REACTION OF 2-AMINO-4(3H)-PYRIMIDINONE WITH CHLOROFORMYL ISOCYANATE
    SAWADA, M
    TANAKA, T
    FURUKAWA, Y
    TODA, T
    TAKAI, Y
    HANAFUSA, T
    BULLETIN OF THE CHEMICAL SOCIETY OF JAPAN, 1988, 61 (06) : 2217 - 2219
  • [42] A SIMPLE, REGIOSELECTIVE SYNTHESIS OF 5,6-DIHYDRO-1,3,5-TRIAZINE-2,4(1H,3H)-DIONE DERIVATIVES FROM N-TRIMETHYLSILYL IMINES VIA 1,3-DIAZABUTADIENES
    BARLUENGA, J
    TOMAS, M
    BALLESTEROS, A
    LOPEZ, LA
    SYNTHESIS-STUTTGART, 1989, (03): : 228 - 229
  • [43] A novel and environmentally benign synthesis of 1,3-disubstituted-(1H,3H)- pyrimidine-2,4-diones
    Ramana, M.M.V.
    Pawar, Sanjay C.
    Journal of Chemical and Pharmaceutical Research, 2014, 6 (02) : 525 - 531
  • [44] ELECTRON-IMPACT INDUCED FRAGMENTATION OF 3-HYDROXY QUINAZOLINE-2,4(1H,3H)DIONE, PYRIDOPYRIMIDINE-2,4(1H,3H)DIONES, LUMAZINE AND ALLOXAZINE
    TSERNG, KY
    BELL, CL
    BAUER, L
    JOURNAL OF HETEROCYCLIC CHEMISTRY, 1975, 12 (01) : 79 - 83
  • [45] Synthesis, biological evaluation and molecular docking of 3-substituted quinazoline-2,4(1H, 3H)-diones
    Lumadhar Santos-Ballardo
    Fernando García-Páez
    Lorenzo A Picos-Corrales
    Adrián Ochoa-Terán
    Pedro Bastidas
    Loranda Calderón-Zamora
    Guadalupe Rendón-Maldonado
    Ulises Osuna-Martínez
    Juan I Sarmiento-Sánchez
    Journal of Chemical Sciences, 2020, 132
  • [46] Synthesis, biological evaluation and molecular docking of 3-substituted quinazoline-2,4(1H, 3H)-diones
    Santos-Ballardo, Lumadhar
    Garcia-Paez, Fernando
    Picos-Corrales, Lorenzo A.
    Ochoa-Teran, Adrian
    Bastidas, Pedro
    Calderon-Zamora, Loranda
    Rendon-Maldonado, Guadalupe
    Osuna-Martinez, Ulises
    Sarmiento-Sanchez, Juan, I
    JOURNAL OF CHEMICAL SCIENCES, 2020, 132 (01)
  • [47] A NOVEL SYNTHESIS OF PYRIDO [1,2-A] 1,3,5-TRIAZINE-2,4-DITHIONES
    JOSHUA, CP
    THOMAS, SK
    HETEROCYCLES, 1982, 19 (03) : 531 - 534
  • [48] Insertion of Ethyl Isocyanate at the Tungsten–Chlorine Bond. Crystal Structure of 1,3,5-Triethyl-1,3,5-triazine-2,4,6-(1H,3H,5H)-trione
    N. A. Ovchinnikova
    A. E. Sinyakov
    A. M. Reznik
    S. G. Sakharov
    Yu. E. Gorbunova
    Yu. N. Mikhailov
    A. S. Kanishcheva
    V. D. Butskii
    Russian Journal of Coordination Chemistry, 2002, 28 : 673 - 677
  • [49] 3-aryl(alkyl)quinazoline-2,4(1H,3H)-diones and their alkyl derivatives
    A. S. Shestakov
    O. E. Sidorenko
    I. S. Bushmarinov
    Kh. S. Shikhaliev
    M. Yu. Antipin
    Russian Journal of Organic Chemistry, 2009, 45 : 1691 - 1696
  • [50] 3-Aryl(alkyl)quinazoline-2,4(1H,3H)-diones and Their Alkyl Derivatives
    Shestakov, A. S.
    Sidorenko, O. E.
    Bushmarinov, I. S.
    Shikhaliev, Kh. S.
    Antipin, M. Yu.
    RUSSIAN JOURNAL OF ORGANIC CHEMISTRY, 2009, 45 (11) : 1691 - 1696