Oxovanadium(IV) Complex with 1-Hydroxyethane-1,1-Diphosphonic Acid and Bis(2-pyridyl-1,2,4-Triazol-3-yl)methane

被引：0
|
作者：
Shul'gin, V. F. [1 ]
Baluda, Yu, I [1 ]
Gusev, A. N. [1 ]
Kryukova, M. A. [2 ]
机构：
[1] Vernadsky Crimean Fed Univ, Simferopol, Russia
[2] St Petersburg State Univ, Inst Chem, St Petersburg, Russia
来源：
RUSSIAN JOURNAL OF COORDINATION CHEMISTRY | 2021年 / 47卷 / 03期
基金：
俄罗斯科学基金会;
关键词：
oxovanadium(IV); spacered; 1; 2; 4-triazole; X-ray diffraction analysis;
D O I：
10.1134/S1070328421030052
中图分类号：
O61 [无机化学];
学科分类号：
070301 ; 081704 ;
摘要：
The synthesis of oxovanadium(IV) complex with 1-hydroxyethane-1,1-diphosphonic acid (H4EDP) anion and bis(2-pyridyl-1,2,4-triazol-3-yl)methane (H2L) is described. The reaction of VOSO4 with H4EDP and H2L followed by neutralization of the reaction mixture with Et3N gives the trinuclear complex [(VO)(4)(H2L)(2)(EDP)(2)(H2O)(2)]center dot 4H(2)O (I), which was studied by IR and ESR spectroscopy. The molecular and crystal structures of complex I were determined by X-ray diffraction (CIF file CCDC no. 2022772).
引用
收藏
页码：204 / 208
页数：5
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