Synthesis and spectroscopic characterization of transition metal(II) complexes with a novel N2O2 donor ligand

被引:3
|
作者
Baysal, A. [1 ]
Buldag, A. [1 ]
机构
[1] Univ Dicle, Fac Sci & Art, Dept Chem, Diyarbakir, Turkey
关键词
D O I
10.1134/S1070328407030062
中图分类号
O61 [无机化学];
学科分类号
070301 ; 081704 ;
摘要
A novel tetradentate Schiff base ligand, 2,2'-{1,2-phenylene-bis[(E)-methylidienenitrilo]}dipyridine-3-ol, has been synthesized by the condensation of phthalaldehyde with 2-amino-3-hydroxypyridine. A series of its complexes with transition metals have been prepared and characterized by a combination of IR, UV-VIS, and LC-MS spectroscopy, magnetic measurements, and elemental analyses. The spectral data of the ligand and its complexes are discussed in connection with structural changes that occur due to complexation.
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页码:190 / 193
页数:4
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