3,4a-Dichloro-10a-(3-chloro-6-hydroxy-2,2,6-trimethylcyclohexylmethyl)-6,8-dihydroxy-2,2,7-trimethyl-3,4,4a,10a-tetrahydro-2H-benzo[g]chromene-5,10-dione

被引：11

作者：

Soria-Mercado, IE

Jensen, PR

Fenical, W

Kassel, S

Golen, J

机构：

[1] Univ Autonoma Baja California, Fac Ciencias Marinas, Ensenada 22800, Baja California, Mexico

[2] Univ Calif San Diego, Scripps Inst Oceanog, Ctr Marine Biotechnol & Biomed, La Jolla, CA 92093 USA

[3] Univ Calif San Diego, Dept Chem & Biochem, La Jolla, CA 92093 USA

[4] Villanova Univ, Dept Chem, Villanova, PA 19085 USA

[5] Univ Massachusetts, Dept Chem & Biochem, N Dartmouth, MA 02747 USA

来源：

ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS | 2004年 / 60卷

关键词：

D O I：

10.1107/S1600536804020094

中图分类号：

O7 [晶体学];

学科分类号：

0702 ; 070205 ; 0703 ; 080501 ;

摘要：

The title microbial antibiotic, C26H33Cl3O6, is an unusual trichlorinated dihydroquinone with cyclized prenyl and geranyl terpene substitution. The crystal structure provides an unambiguous assignment for this compound including its absolute stereochemistry, and shows the favored configuration of the chlorocyclohexane substituent.

引用

页码：O1627 / O1629

页数：3

共 35 条

[31] SYNTHESIS AND SPECTROSCOPIC CHARACTERIZATIONS OF BOTH 1-ETHYL-4,8-DIHYDRO-10-METHOXY-3-METHYL-8-R(1)-6-R(2)-DIPYRAZOLO[3,4-B/4',3'-F][1,5]DIAZOCIN-5(1H)-ONES AND 1-ETHYL-1,4,8,9-TETRAHYDRO-3,9-DIMETHYL-8-R(1)-6-R(2)-DIPYRAZOLO[3,4-B/4',3'-F][1,5]DIAZOCINE-5,10-DIONES OF PHARMACEUTICAL INTEREST
MIGLIARA, O
LAMARTINA, L
RAINIERI, R
JOURNAL OF HETEROCYCLIC CHEMISTRY, 1995, 32 (05) : 1589 - 1593
[32] Synthesis and Spectroscopic Characterizations of both 1-Ethyl-4,8-dihydro-10-methoxy-3 methyl 8 R1-6-R2-dipyrazolo[3,4-b:4',3'-f$ RB@-[ 1,5]dianocin-5(1H)-ones and 1-Ethyl-1,4,8,9-tetrahydro-3,9-dimethy-8 -R1$ MIN@6-R2-dipyrazolo[3,4-b:4',3'-f][ 1,5] diazocine-5,10-diones of Pharmaceutical Interest
Migliara, O.
Lamartina, L.
Rainieri, R.
Journal of Heterocyclic Chemistry,
[33] Five-membered 2,3-dioxoheterocycles: LXIV. Reactions of 1-methyl-3,4-dihydroisoquinolines with 5-arylfuran-2,3-diones and (Z)-alkyl 4-aryl-2-hydroxy-4-oxobut-2-enoates. Crystal and molecular structure of (2Z,5Z)-3-hydroxy-5-{8,8-dimethyl-2,3,8,9-tetrahydro[1,4]dioxino[2,3-g]isoquinolin-6(7H)-ylidene}-1-phenylpent-2-ene-1,4-dione
Khalturina, V. V.
Shklyaev, Yu. V.
Aliev, Z. G.
Maslivets, A. N.
RUSSIAN JOURNAL OF ORGANIC CHEMISTRY, 2009, 45 (05) : 728 - 734
[34] Five-membered 2,3-dioxoheterocycles: LXIV. Reactions of 1-methyl-3,4-dihydroisoquinolines with 5-arylfuran-2,3-diones and (Z)-alkyl 4-aryl-2-hydroxy-4-oxobut-2-enoates. Crystal and molecular structure of (2Z,5Z)-3-hydroxy-5-{8,8-dimethyl-2,3,8,9-tetrahydro[1,4]dioxino[2,3-g]isoquinolin-6(7H)-ylidene}-1-phenylpent-2-ene-1,4-dione
V. V. Khalturina
Yu. V. Shklyaev
Z. G. Aliev
A. N. Maslivets
Russian Journal of Organic Chemistry, 2009, 45 : 728 - 734
[35] Further studies on polycyclic arene sulfides.: Preparation and mutagenic activity of 9,10,10a,11a-tetrahydrotriphenyleno[1,2-b]thiirene, 1a,2,3,10b-tetrahydro-5H-thiereno[3,4]benzo[1,2-b]fluorene and 1a,2,3,11b-tetrahydroacenaphtho[1′,2′:6,7] naphth[1,2-b] thiirene
Blum, J
Kogan, V
Glatt, H
JOURNAL OF HETEROCYCLIC CHEMISTRY, 2000, 37 (05) : 1109 - 1112

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