Reflector Selection for the Indexing of Electron Backscatter Diffraction Patterns

被引:5
|
作者
Wright, Stuart, I [1 ]
Singh, Saransh [2 ,3 ]
De Graef, Marc [3 ]
机构
[1] EDAX, 392 East 12300 South,Suite H, Draper, UT 84020 USA
[2] Lawrence Livermore Natl Lab, 7000 East Ave, Livermore, CA 94550 USA
[3] Carnegie Mellon Univ, Dept Mat Sci & Engn, 5000 Forbes Ave, Pittsburgh, PA 15213 USA
关键词
dynamical simulations; EBSD; electron backscatter diffraction; indexing; FOCK X-RAY; SCATTERING FACTORS;
D O I
10.1017/S1431927619000333
中图分类号
T [工业技术];
学科分类号
08 ;
摘要
We propose a new methodology for ranking the reflectors used in traditional Hough-based indexing of electron backscatter diffraction (EBSD) patterns. Instead of kinematic X-ray or electron structure factors (F-hkl) currently utilized, we propose the integrated Kikuchi band intensity parameter (beta(hkl)) based on integrated dynamical electron backscatter intensities. The proposed parameter is compared with the traditional kinematical intensity, I-hkl(HSP), as well as the average Hough transform peak intensity, and used to index EBSD patterns for a number of different material systems of varying unit cell complexities including nickel, silicon, rutile, and forsterite. For elemental structures, beta(hkl) closely follows the kinematical ranking. However, significant ranking differences arise for more complex unit cells, with the beta(hkl) parameter showing a better correlation with the integrated Hough intensities. Finally, Hough-based indexing of a simulated forsterite data set showed an appreciable improvement in the median confidence index (0.15 to 0.35) when beta(hkl) is used instead of I-hkl(kin) for ranking the reflectors.
引用
收藏
页码:675 / 681
页数:7
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