Anisotropic threshold stress intensity factor, KIH and crack growth rate in delayed hydride cracking of Zr-2.5Nb pressure tubes

The objectives of this study are to systematically investigate the delayed hydride cracking (DHC) velocity and the threshold-stress intensity factor, K-IH, of a Zr-2.5Nb pressure tube as a function of orientation and elucidate the cause of this anistropic DHC behavior. The DHC velocity as a function of orientation was determined using flattened cantilever beam specimens with 60 ppm H while the threshold-stress intensity factor K-IH, was evaluated as a function of orientation on the curved compact-tension (CT) and cantilever-beam (CB) specimens charged with hydrogen to 200 ppm H. To infer a difference in a stress gradient ahead of the crack tip as a function of orientation, tensile tests were conducted at temperatures ranging from room temperature (RT) to 560 degreesC using small tensile specimens of 2-mm-gage length taken from three directions of the tube. A textural change was investigated by comparing the inverse pole figures before and after DHC while the 110171 pole figures were constructed to find out the growth pattern of the DHC crack as a function of orientation. Faster DHC velocity and lower K,H were obtained over temperatures of 170 degreesC to 270 degreesC, when the DHC crack grew in the longitudinal direction of the Zr-2.5Nb pressure tube. The strain hardening after yielding and the extent of the textural change accompanied by DHC were higher in the longitudinal direction of the tube, suggesting a higher stress gradient ahead of the crack tip. Thus, the anisotropic DHC behavior of a Zr-2.5Nb pressure tube is discussed based on the stress gradient ahead of the crack tip governed by strain-hardening rate after yielding and a change in texture accompanied by DHC, and the distribution of the 110171 hydride habit planes.