Hilic MS/MS determination of amino acids in herbs of Fumaria schleicheri L., Ocimum basilicum L., and leaves of Corylus avellana L.

被引:7
|
作者
Prokopenko, Yuliya [1 ]
Jakstas, Valdas [2 ]
Zvikas, Vaidotas [2 ]
Georgiyants, Victoriya [3 ]
Ivanauskas, Liudas [4 ]
机构
[1] Natl Univ Pharm, Dept Qual Standardisat & Certificat Drugs, Kharkov, Ukraine
[2] Lithuanian Univ Hlth Sci, Med Acad, Dept Pharmacognosy, Fac Pharm, Kaunas, Lithuania
[3] Natl Univ Pharm, Dept Pharmaceut Chem, Kharkov, Ukraine
[4] Lithuanian Univ Hlth Sci, Med Acad, Dept Analyt & Toxicol Chem, Fac Pharm, Kaunas, Lithuania
关键词
Amino acids; Fumaria schleicheri L; Ocimum basilicum L; Corylus avellana L; HILIC MS; MS;
D O I
10.1080/14786419.2018.1477145
中图分类号
O69 [应用化学];
学科分类号
081704 ;
摘要
The aim of research was to study the content of amino acids using in extracts of Fumaria schleicheri L., Ocimum basilicum L., and Corylus avellana L. by HILIC MS/MS method. Separation of amino acids in the samples was carried out with Acquity H-class UPLC system (Waters, Milford, USA) equipped with SeQuant ZIC-Hilic collumn (2.1 x 150 mm, 3.5 mu m) (Merck Millipore, Darmstadt, Germany). The MS/MS fragment ion chromatograms of the test solutions established the presence of 19 amino acids. The obtained results have shown that O. basilicum L. characterized the highest concentrations of different neurogenic amino acids (128.1 mg/kg), comparing with F. schleicheri L. and C. avellana L. (57.72 and 52.91 mg/kg, respectively). [GRAPHICS] .
引用
收藏
页码:1961 / 1963
页数:3
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