Synthesis, X-ray structure and N-H...O interactions in 1,3-diphenyl-urea

被引：16
|
作者：
Rajnikant [1 ]
Dinesh
Deshmukh, M. B.
Kamni
机构：
[1] Univ Jammu, PG Dept Phys, Jammu 180006, India
[2] Shivaji Univ, Dept Chem, Kolhapur 416004, Maharashtra, India
来源：
BULLETIN OF MATERIALS SCIENCE | 2006年 / 29卷 / 03期
关键词：
alkaloids; X-ray structure; diffractometer; hydrogen bond;
D O I：
10.1007/BF02706491
中图分类号：
T [工业技术];
学科分类号：
08 ;
摘要：
The synthesis, X-ray structure and role of intermolecular interactions have been studied in case of 1,3-diphenyl-urea, owing to its medicinal importance. The compound crystallizes in orthorhombic crystal system (space group, Pna2(1)) with unit cell parameters, a = 9(.)118(3), b = 10(.)558(2), c = 11(.)780(3) angstrom and Z = 4. The structure has been solved by direct methods and refined to a final R-value of 0.0316. The oxygen atom of the carbonyl group is responsible for the existence of two N-H(...)0 intermolecular interactions.
引用
收藏
页码：239 / 242
页数：4
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