Chemical transformations of lanthanide nitrate complexes: Synthesis and X-ray diffraction analysis

被引：3

作者：

Novitskii, G. ^{[1
]}

Borta, A. ^{[2
]}

Ganzhu, D. ^{[3
]}

Shova, S. ^{[2
]}

Filippova, I. G. ^{[2
]}

Simonov, Yu. A. ^{[2
]}

机构：

[1] Moldavian Acad Sci, Inst Chem, Kishinev, Moldova

[2] Moldavian Acad Sci, Inst Appl Phys, Kishinev, Moldova

[3] Cuza Univ, Iasi, Romania

来源：

RUSSIAN JOURNAL OF COORDINATION CHEMISTRY | 2009年 / 35卷 / 05期

基金：

俄罗斯基础研究基金会;

关键词：

BOND-VALENCE PARAMETERS;

D O I：

10.1134/S107032840905011X

中图分类号：

O61 [无机化学];

学科分类号：

070301 ; 081704 ;

摘要：

The complexes [Dy(NO3)(3)(Bipy)(2)], (HBipy)[Gd(NO3)(4)(Bipy)], and [Fe-III(Me(2)Bipy)(3)][La(NO3)(5)(H2O)]NO3 and the precursor of the latter, [(FePc2)-Pc-II(Me(2)Bipy)](CHCl3) center dot 1.5H(2)O (where Bipy is the 2,2'-bipyridyl, Me(2)Bipy is the 4,4'-dimethyl-2,2'-bipyridyl, and Pc- is the pyridine-2-carboxylate anion), were obtained and characterized by X-ray diffraction analysis. Depending on the conditions of the synthesis and the reagents, the number of coordinated nitrate groups in the lanthanide complex increases from three to five: [Dy(NO3)(3)(Bipy)(2)], [Gd(NO3)(4)(Bipy)](-), and [La(NO3)(5)(H2O)](2-).

引用

页码：381 / 388

页数：8

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