A device for the application of uniaxial strain to single crystal samples for use in synchrotron radiation experiments

被引：8

作者：

Gannon, L. ^{[1
,2
]}

Bosak, A. ^{[3
]}

Burkovsky, R. G. ^{[3
,4
]}

Nisbet, G. ^{[2
]}

Petrovic, A. P. ^{[5
]}

Hoesch, M. ^{[2
]}

机构：

[1] Univ Oxford, Dept Phys, Clarendon Lab, Oxford OX1 3PU, England

[2] Diamond Light Source, Didcot OX11 ODE, Oxon, England

[3] European Synchrotron Radiat Facil, F-38043 Grenoble, France

[4] Peter Great St Petersburg Polytech Univ, St Petersburg 195251, Russia

[5] Univ Geneva, DPMC MaNEP, CH-1211 Geneva 4, Switzerland

来源：

REVIEW OF SCIENTIFIC INSTRUMENTS | 2015年 / 86卷 / 10期

基金：

英国工程与自然科学研究理事会;

关键词：

Strain - Temperature - Synchrotron radiation - Synchrotrons - Cesium compounds - Potassium compounds - Single crystals - X ray diffraction - X ray scattering - Molybdenum compounds;

D O I：

10.1063/1.4933383

中图分类号：

TH7 [仪器、仪表];

学科分类号：

0804 ; 080401 ; 081102 ;

摘要：

We present the design, construction, and testing of a straining device compatible with many different synchrotron radiation techniques, in a wide range of experimental environments (including low temperature, high field and ultra-high vacuum). The device has been tested by X-ray diffraction on single crystal samples of quasi-one-dimensional Cs2Mo6Se6 and K2Mo6Se6, in which microscopic strains up to a Delta c/c = 0.12% +/- 0.01% change in the c lattice parameters have been achieved. We have also used the device in an inelastic X-ray scattering experiment, to probe the strain-dependent speed of sound. along the c axis. A reduction Delta v/v of up to -3.8% was obtained at a strain of Delta c/c = 0.25% in K2Mo6Se6. (C) 2015 AIP Publishing LLC.

引用

页数：7

共 50 条

[1] Observation by synchrotron radiation of deformation behaviour in single-crystal Cu under uniaxial tension
Kim, KH
Koo, YM
Chang, YW
PHILOSOPHICAL MAGAZINE LETTERS, 1998, 77 (02) : 83 - 88
[2] NEW OPPORTUNITIES IN SINGLE-CRYSTAL AND POWDER DIFFRACTION EXPERIMENTS USING SYNCHROTRON RADIATION
BERAR, JF
BESSIERE, M
LEFEBVRE, S
JOURNAL DE CHIMIE PHYSIQUE ET DE PHYSICO-CHIMIE BIOLOGIQUE, 1989, 86 (7-8) : 1473 - 1489
[3] Microdiffraction experiments on single polymeric fibers by synchrotron radiation
European Synchrotron Radiation, Facility, Grenoble, France
Macromolecules, 4 (1033-1037):
[4] Microdiffraction experiments on single polymeric fibers by synchrotron radiation
Riekel, C
Cedola, A
Heidelbach, F
Wegner, K
MACROMOLECULES, 1997, 30 (04) : 1033 - 1037
[5] Application of a portable pulsed magnet to synchrotron radiation experiments
Matsuda, YH
Ueda, Y
Nojiri, H
Takahashi, T
Inami, T
Ohwada, K
Murakami, Y
Arima, T
PHYSICA B-CONDENSED MATTER, 2004, 346 : 519 - 523
[6] Application of synchrotron radiation technique to analysis of environmental samples
Zaw, M
Szymczak, R
Twining, J
NUCLEAR INSTRUMENTS & METHODS IN PHYSICS RESEARCH SECTION B-BEAM INTERACTIONS WITH MATERIALS AND ATOMS, 2002, 190 : 856 - 859
[7] Contamination experiments for Mo/Si multilayer mirrors with the use of single-bunch synchrotron radiation
Niibe, Masahito
Koida, Keigo
Kakutani, Yukinobu
11TH INTERNATIONAL CONFERENCE ON SYNCHROTRON RADIATION INSTRUMENTATION (SRI 2012), 2013, 425
[8] Single photon counting pixel detectors for synchrotron radiation experiments
Toyokawa, H.
Broennimann, Ch.
Eikenberry, E. F.
Henrich, B.
Kawase, M.
Kobas, M.
Kraft, P.
Sato, M.
Schmitt, B.
Suzuki, M.
Tanida, H.
Uruga, T.
NUCLEAR INSTRUMENTS & METHODS IN PHYSICS RESEARCH SECTION A-ACCELERATORS SPECTROMETERS DETECTORS AND ASSOCIATED EQUIPMENT, 2010, 623 (01): : 204 - 206
[9] Movement of Single-Crystal Protein Samples at Synchrotron Beamlines
Rotella, Frank J.
Alkire, Randy W.
Duke, Norma E. C.
ACTA CRYSTALLOGRAPHICA A-FOUNDATION AND ADVANCES, 2005, 61 : C137 - C137
[10] Effect of strain in crystal on the forbidden reflections in the resonant diffraction of synchrotron radiation
G. T. Mulyavko
E. N. Ovchinnikova
A. P. Oreshko
V. E. Dmitrienko
E. Kh. Mukhamedzhanov
Crystallography Reports, 2012, 57 : 18 - 23

← 1 2 3 4 5 →