Recovery and Purification of Nicotine from Waste Tobacco by Aqueous Two-Phase System/Reverse Extraction

被引：1
|
作者：
Xing, Jian-min [1 ]
Li, Fen-fang [1 ]
Ping, Jing [2 ]
机构：
[1] Cent S Univ, Sch Chem & Chem Engn, Changsha 410083, Peoples R China
[2] Mem Univ Newfoundland, Fac Engn & Appl Sci, St John, NF A1B 3X5, Canada
来源：
NATURAL PRODUCT COMMUNICATIONS | 2009年 / 4卷 / 08期
关键词：
nicotine; aqueous two-phase separation; purification; reverse extraction; extraction kinetics;
D O I：
暂无
中图分类号：
R914 [药物化学];
学科分类号：
100701 ;
摘要：
A two-step process has been developed for the purification of nicotine from waste tobacco using an aqueous two-phase system and solvent reverse extraction. The partitioning behavior of nicotine was investigated in an isopropyl alcohol/(NH4)(2)SO4 aqueous two-phase system. The effects of the addition of salt, pH and temperature on the partitioning behavior of nicotine were studied. The recovery rate of nicotine was 96.1% with a purity of above 99% when optimal conditions were used [(NH4)(2)SO4 25%, pH 9, temperature 35 degrees C, isopropyl alcohol 5 mL].
引用
收藏
页码：1093 / 1094
页数：2
相关论文
共 50 条
  • [21] Simultaneous extraction and purification of polysaccharides and proteins from Pleurotus ostreatus using an aqueous two-phase system
    Yang, Zhilai
    Wang, Jingkun
    Wang, Hongyu
    Xie, Huixian
    Zhang, Yingnan
    Wang, Meng
    JOURNAL OF FOOD SCIENCE, 2025, 90 (01)
  • [22] Extraction and purification of Polyhydroxyalkanoates (PHAs): application of Thermoseparating aqueous two-phase extraction
    Yoong Kit Leong
    Pau Loke Show
    John Chi-Wei Lan
    Hwei-San Loh
    Yee Jiun Yap
    Tau Chaun Ling
    Journal of Polymer Research, 2017, 24
  • [23] Extraction and purification of Polyhydroxyalkanoates (PHAs): application of Thermoseparating aqueous two-phase extraction
    Leong, Yoong Kit
    Show, Pau Loke
    Lan, John Chi-Wei
    Loh, Hwei-San
    Yap, Yee Jiun
    Ling, Tau Chaun
    JOURNAL OF POLYMER RESEARCH, 2017, 24 (10)
  • [24] Copper recovery from ore by liquid-liquid extraction using aqueous two-phase system
    de Lemos, Leandro Rodrigues
    Boggione Santos, Igor Jose
    Rodrigues, Guilherme Dias
    Mendes da Silva, Luis Henrique
    Hespanhol da Silva, Maria C.
    JOURNAL OF HAZARDOUS MATERIALS, 2012, 237 : 209 - 214
  • [25] Separation and purification of laccases from two different fungi using aqueous two-phase extraction
    Prinz, Axel
    Hoenig, Jacqueline
    Schuettmann, Ina
    Zorn, Holger
    Zeiner, Tim
    PROCESS BIOCHEMISTRY, 2014, 49 (02) : 335 - 346
  • [26] Aqueous two-phase system for citrinin extraction from fermentation broth
    Pimentel, M. C. B.
    Araujo, A. I.
    Figueiredo, Z. M. B.
    Silva, R. A.
    Cavalcanti, M. T. H.
    Moreira, K. A.
    Filho, J. L. L.
    Porto, A. L. F.
    SEPARATION AND PURIFICATION TECHNOLOGY, 2013, 110 : 158 - 163
  • [27] Collection and purification of parasporal crystals from Bacillus thuringiensis by aqueous two-phase extraction
    Lin, DQ
    Yao, SJ
    Mei, LH
    Zhu, ZQ
    SEPARATION SCIENCE AND TECHNOLOGY, 2003, 38 (07) : 1665 - 1680
  • [28] Extraction and Recovery of Rutin from Acerola Waste using Alcohol-Salt-Based Aqueous Two-Phase Systems
    Reis, Igor A. O.
    Santos, Samuel B.
    Pereira, Frances D. S.
    Sobral, Carla R. S.
    Freire, Mara G.
    Freitas, Lisiane S.
    Soares, Cleide M. F.
    Lima, Alvaro S.
    SEPARATION SCIENCE AND TECHNOLOGY, 2014, 49 (05) : 656 - 663
  • [29] Hexafluoroisopropanol-salt aqueous two-phase system for extraction and purification of chlorogenic acid from ramie leaves
    Huang, Anqi
    Deng, Wenwen
    Wu, Dandan
    Wu, Shuwen
    Xiao, Yuxiu
    JOURNAL OF CHROMATOGRAPHY A, 2019, 1597 : 196 - 201
  • [30] Recovery of isoamylase using an aqueous two-phase system
    Jinn-Tsyy Lai
    Min-Hui Chen
    Hung-Yun Wan
    Chii-Cherng Liao
    JOURNAL OF THE CHINESE INSTITUTE OF CHEMICAL ENGINEERS, 2006, 37 (02): : 107 - 115
12345