Recovery and Purification of Nicotine from Waste Tobacco by Aqueous Two-Phase System/Reverse Extraction

被引：1
|
作者：
Xing, Jian-min [1 ]
Li, Fen-fang [1 ]
Ping, Jing [2 ]
机构：
[1] Cent S Univ, Sch Chem & Chem Engn, Changsha 410083, Peoples R China
[2] Mem Univ Newfoundland, Fac Engn & Appl Sci, St John, NF A1B 3X5, Canada
来源：
NATURAL PRODUCT COMMUNICATIONS | 2009年 / 4卷 / 08期
关键词：
nicotine; aqueous two-phase separation; purification; reverse extraction; extraction kinetics;
D O I：
暂无
中图分类号：
R914 [药物化学];
学科分类号：
100701 ;
摘要：
A two-step process has been developed for the purification of nicotine from waste tobacco using an aqueous two-phase system and solvent reverse extraction. The partitioning behavior of nicotine was investigated in an isopropyl alcohol/(NH4)(2)SO4 aqueous two-phase system. The effects of the addition of salt, pH and temperature on the partitioning behavior of nicotine were studied. The recovery rate of nicotine was 96.1% with a purity of above 99% when optimal conditions were used [(NH4)(2)SO4 25%, pH 9, temperature 35 degrees C, isopropyl alcohol 5 mL].
引用
收藏
页码：1093 / 1094
页数：2
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