Synthesis and spectroscopic properties of 15N-labelled 1,2,4-thiadiazoles

被引:6
|
作者
Pavlik, JW [1 ]
Changtong, C
Tantayanon, S
机构
[1] Worcester Polytech Inst, Dept Chem & Biochem, Worcester, MA 01609 USA
[2] Chulalongkorn Univ, Dept Chem, Bangkok 10330, Thailand
关键词
D O I
10.1002/jhet.5570390135
中图分类号
O62 [有机化学];
学科分类号
070303 ; 081704 ;
摘要
5-Phenyl-1,2,4-thiadiazole-4-N-15 and 3-methyl-5-phenyl-1,2,4-tlliadiazole-4-N-15 were synthesized from commercially available benazmide-N-15. The mass spectra and the H-1, C-13, and N-15-nmr spectra of these compounds, which show various long-range heteronuclear coupling with the N-15-nucleus, are discussed.
引用
收藏
页码:237 / 239
页数:3
相关论文
共 50 条
  • [21] Synthesis and thermal decomposition of 15N-labelled NTO
    Fan, Leimin
    Dass, Chhabil
    Burkey, Theodore J.
    Journal of Labelled Compounds and Radiopharmaceuticals, 1996, 38 (01) : 87 - 94
  • [22] Synthesis of substituted 1,2,4-triazoles and 1,3,4-thiadiazoles
    Hovsepian, TR
    Dilanian, ER
    Engoian, AP
    Melik-Ohanjanian, RG
    KHIMIYA GETEROTSIKLICHESKIKH SOEDINENII, 2004, (09): : 1377 - 1381
  • [23] Copper(II)-Mediated Homocoupling of Thioamides for the Synthesis of 1,2,4-Thiadiazoles
    Sun, Yadong
    Wu, Wanqing
    Jiang, Huanfeng
    EUROPEAN JOURNAL OF ORGANIC CHEMISTRY, 2014, 2014 (20) : 4239 - 4243
  • [24] Synthesis of substituted 1,2,4-triazoles and 1,3,4-thiadiazoles
    Hovsepian T.R.
    Dilanian E.R.
    Engoyan A.P.
    Melik-Ohanjanian R.G.
    Chemistry of Heterocyclic Compounds, 2004, 40 (09) : 1194 - 1198
  • [25] New synthesis of 5-cyano-1,2,4-thiadiazoles
    Iwakawa, T
    Murabayashi, A
    HETEROCYCLES, 1999, 51 (04) : 811 - 819
  • [26] AMIDRAZONES .6. SYNTHESIS OF 1,2,4-THIADIAZOLES BY THERMOLYSIS OF N-3-THIOCARBAMOYLAMIDRAZONE YLIDES
    SMITH, RF
    FELTZ, TP
    JOURNAL OF HETEROCYCLIC CHEMISTRY, 1981, 18 (01) : 201 - 203
  • [27] Novel 1,2,4-Thiadiazoles with an NO-Producing Fragment
    Serkov, I. V.
    Proshin, A. N.
    Petrova, L. N.
    Bachurin, S. O.
    DOKLADY CHEMISTRY, 2010, 435 : 311 - 313
  • [28] MASS-SPECTRA OF SOME 1,2,4-THIADIAZOLES
    POTTS, KT
    ARMBRUST.R
    JOURNAL OF HETEROCYCLIC CHEMISTRY, 1972, 9 (03) : 651 - &
  • [29] An Expeditious Ultrasound-Initiated Green Synthesis of 1,2,4-Thiadiazoles in Water
    Chauhan, Swati
    Verma, Pratibha
    Mishra, Ankush
    Srivastava, Vandana
    CHEMISTRY OF HETEROCYCLIC COMPOUNDS, 2020, 56 (01) : 123 - 126
  • [30] Novel 1,2,4-thiadiazoles with an NO-producing fragment
    I. V. Serkov
    A. N. Proshin
    L. N. Petrova
    S. O. Bachurin
    Doklady Chemistry, 2010, 435 : 311 - 313