Determination of polyaromatic hydrocarbons in coal tar pitch

被引：15
|
作者：
Afanasov, I. M. [1 ]
Kepman, A. V. [1 ]
Morozov, V. A. [1 ]
Seleznev, A. N. [1 ]
Avdeev, V. V. [1 ]
机构：
[1] Moscow MV Lomonosov State Univ, Dept Chem, Moscow 119992, Russia
来源：
JOURNAL OF ANALYTICAL CHEMISTRY | 2009年 / 64卷 / 04期
关键词：
POLYCYCLIC AROMATIC-HYDROCARBONS; POLYCHLORINATED-BIPHENYLS; EXTRACTION PROCEDURE; MASS-SPECTROMETRY; DEGRADATION; AIR; SEDIMENTS; WATERS; GC/MS; MODEL;
D O I：
10.1134/S1061934809040078
中图分类号：
O65 [分析化学];
学科分类号：
070302 ; 081704 ;
摘要：
Different techniques for extracting polyaromatic hydrocarbons (PAHs) from coal tar pitch for their quantitative determination by gas chromatography-mass spectrometry are compared. It has been found that the ultrasonic treatment of a sample allowed the quantitative extraction of PAHs from coal tar pitch. The results of the quantitative determination of PAHs in samples of coal tar pitch obtained by Soxhlet extraction and liquid-liquid extraction with ultrasonic treatment agree within the experimental error range.
引用
收藏
页码：361 / 365
页数：5
相关论文
共 50 条
  • [41] Sequential Extraction of Coal Tar Pitch and Structural Characterization of Enriched Large Polycyclic Aromatic Hydrocarbons
    Fan, Xiao-Hua
    Li, Wei
    Chen, Lei
    Ouyang, Ting
    Fei, Youqing
    CHEMISTRYSELECT, 2019, 4 (17): : 4874 - 4882
  • [42] PROBLEMS OF ISOLATION AND DETERMINATION OF POLYAROMATIC HYDROCARBONS
    SMIDL, P
    POSPISIL, M
    PECKA, K
    CHEMICKE LISTY, 1989, 83 (01): : 11 - 28
  • [43] Synthetic and Industrial Coal-Tar Pitch and Pitch Coke
    A. I. Simachko
    A. V. Lakhin
    A. N. Timofeev
    S. V. Taschilov
    A. E. Dvoretskiy
    R. T. Latypov
    I. V. Moskalev
    D. M. Kiselkov
    Coke and Chemistry, 2022, 65 : 353 - 362
  • [44] Pitch Coke Formation in Carbonization of Coal Tar Pitch.
    Janik, Miroslav
    Hubsch, Jiri
    Kaloc, Miroslav
    Hutnicke listy, 1980, 35 (01): : 3 - 9
  • [45] Synthetic and Industrial Coal-Tar Pitch and Pitch Coke
    Simachko, A. I.
    Lakhin, A. V.
    Timofeev, A. N.
    Taschilov, S. V.
    Dvoretskiy, A. E.
    Latypov, R. T.
    Moskalev, I. V.
    Kiselkov, D. M.
    COKE AND CHEMISTRY, 2022, 65 (08) : 353 - 362
  • [46] The microchemical distinction of coal tar hydrocarbons
    Behrens, H
    RECUEIL DES TRAVAUX CHIMIQUES DES PAYS-BAS ET DE LA BELGIQUE, 1900, 19 : 386 - 397
  • [47] Coal-Tar Hydrocarbons.
    Collin, G.
    Erdoel und Kohle, Erdgas, Petrochemie vereinigt mit Brennstoff-Chemie, 1979, 32 (11): : 512 - 519
  • [48] Organic sulfur compounds of coal tar and coal tar pitch. 1. Types of organic sulfur compounds and methods of their determination
    Yakovleva, T.P.
    Dolzhanskaya, Yu.B.
    Pityulin, I.N.
    Privalova, N.V.
    Gapotchenko, N.P.
    Koks i Khimiya, 1992, (09): : 27 - 31
  • [49] Kinetics of mesophase transformation of coal tar pitch
    Shui, HF
    Feng, YT
    Shen, BX
    Gao, JS
    FUEL PROCESSING TECHNOLOGY, 1998, 55 (02) : 153 - 160
  • [50] Coal-tar pitch production and use
    Tsikarev, D.A.
    Koks i Khimiya, 1995, (01): : 37 - 38
12345