THE SYNTHESIS OF DIPYRAZOLYLMETHANES, X-RAY STRUCTURE ANALYSIS

被引:1
|
作者
Ma, Yuan [1 ]
Wang, Jinxia [1 ]
Ma, Hengchang [1 ]
机构
[1] Northwest Normal Univ, Coll Chem & Chem Engn, Key Lab Polymer Mat Gansu Prov, Key Lab Ecoenvironm Related Polymer Mat,Minist Ed, Lanzhou 730070, Peoples R China
基金
中国国家自然科学基金;
关键词
RUBAZOIC ACID-DERIVATIVES; 4-(5-HYDROXY-4-PYRAZOLYLIMINO)-2-PYRAZOLIN-5-ONES; TRANSFORMATIONS; NUCLEOPHILES; CARBONYLS; OXIDATION; ALCOHOLS; INDOLES;
D O I
10.3987/COM-13-12840
中图分类号
O62 [有机化学];
学科分类号
070303 ; 081704 ;
摘要
A small dipyrazoylmethane compounds library was established via the reaction of 5-alkyl- and 5-aryl-2-aryl-3H-pyrazol-3-ones with DMSO in the presence of NaOAc center dot 3H(2)O as base using LiBr center dot H2O as additive at 100 degrees C.
引用
收藏
页码:1645 / 1655
页数:11
相关论文
共 50 条
  • [21] X-RAY STRUCTURE ANALYSIS OF LAPPACONINE
    BIRNBAUM, GI
    TETRAHEDRON LETTERS, 1969, (26) : 2193 - &
  • [22] SYNTHESIS AND X-RAY ANALYSIS OF DIAMOND
    PUGH, HL
    LEES, J
    BLAND, JA
    NATURE, 1961, 191 (479) : 865 - +
  • [23] First synthesis, X-ray structure analysis and reactions of alkenyltriphenylbismuthonium salts
    Matano, Y
    Yoshimune, M
    Azuma, N
    Suzuki, H
    JOURNAL OF THE CHEMICAL SOCIETY-PERKIN TRANSACTIONS 1, 1996, (16): : 1971 - 1977
  • [24] X-ray analysis of nanowires and nanowire devices: structure, function and synthesis
    Chayanun, Lert
    Benter, Sandra
    Mikkelsen, Anders
    Timm, Rainer
    Wallentin, Jesper
    NANOTECHNOLOGY, 2025, 36 (15)
  • [25] Synthesis and X-ray crystallographic analysis of a bis(arylmethylidene)pyranone structure
    Abaee, M. Saeed
    Mojtahedi, Mohammad M.
    Sharifi, Roholah
    Zahedi, Mohammad M.
    Mesbah, A. Wahid
    Massa, Werner
    JOURNAL OF CHEMICAL RESEARCH, 2008, (07) : 388 - 389
  • [26] On the estimation of the termination effect in Fourier synthesis in X-ray structure analysis
    Takahashi, Y.
    Ohshima, K.
    Yamamoto, K.
    Yukino, K.
    Okamura, F.P.
    Journal of Applied Crystallography, 1998, 31 (pt 6):
  • [27] N-PERFLUOROALKANESULFONYL SULFILIMINES:SYNTHESIS AND X-RAY STRUCTURE ANALYSIS
    Shi Zheng ZHUa
    Ai Wen LI~a
    Kuang WU~b a Shanghai Institute of Organic Chemistry
    ChineseChemicalLetters, 1992, (09) : 703 - 706
  • [28] On the estimation of the termination effect in Fourier synthesis in X-ray structure analysis
    Takahashi, Y
    Ohshima, K
    Yamamoto, K
    Yukino, K
    Okamura, FP
    JOURNAL OF APPLIED CRYSTALLOGRAPHY, 1998, 31 : 917 - 921
  • [29] A stabilized triarylbismuthane imide: Synthesis and first X-ray structure analysis
    Ikegami, T
    Suzuki, H
    ORGANOMETALLICS, 1998, 17 (06) : 1013 - 1017
  • [30] SYNTHESIS AND X-RAY STRUCTURE OF 4'-THIOTHYMIDINE
    UENISHI, J
    TAKAHASHI, K
    MOTOYAMA, M
    AKASHI, H
    CHEMISTRY LETTERS, 1993, (02) : 255 - 256