The structure of uniaxially stretched isotactic polypropylene sheets: Imaging with frequency-modulation atomic force microscopy

被引：4
|
作者：
Uchida, Kiminori [1 ]
Mita, Kazuki [1 ]
Matsuoka, Osamu [1 ]
Isaki, Takeharu [1 ]
Kimura, Kenjiro [2 ]
Onishi, Hiroshi [2 ]
机构：
[1] Mitsui Chem Inc, Adv Anal Lab, 580-32 Nagaura, Chiba 2990265, Japan
[2] Kobe Univ, Grad Sch Sci, Dept Chem, Nada Ku, Kobe, Hyogo 6578501, Japan
来源：
POLYMER | 2016年 / 82卷
关键词：
Frequency-modulation atomic force microscopy; Polypropylene; X-ray scattering; Uniaxial stretching; X-RAY-SCATTERING; CRYSTALS; DEFORMATION; CRYSTALLIZATION; VISUALIZATION; MORPHOLOGY; HYDRATION; BEHAVIOR; LIQUID;
D O I：
10.1016/j.polymer.2015.11.033
中图分类号：
O63 [高分子化学（高聚物）];
学科分类号：
070305 ; 080501 ; 081704 ;
摘要：
Isotactic polypropylene sheets were uniaxially stretched and observed with a frequency-modulation atomic force microscope operated in phenyloctane liquid. Crystalline lamellae were seen in fibrils with their axis parallel to the stretched direction. Individual CH3 side-chains of three-fold helices were identified in the lamellae. Fragmentation of the lamellae was induced by further stretching. The real-space features observed with the microscope were successfully compared with X-ray scattering results obtained in a synchrotron radiation facility. (C) 2015 Elsevier Ltd. All rights reserved.
引用
收藏
页码：349 / 355
页数：7
相关论文
共 50 条
  • [31] Cross-Sectional Imaging of Boundary Lubrication Layer Formed by Fatty Acid by Means of Frequency-Modulation Atomic Force Microscopy
    Hirayama, Tomoko
    Kawamura, Ryota
    Fujino, Keita
    Matsuoka, Takashi
    Komiya, Hiroshi
    Onishi, Hiroshi
    LANGMUIR, 2017, 33 (40) : 10492 - 10500
  • [32] ATOMIC FORCE MICROSCOPY OF POLYMER CRYSTALS .4. IMAGING OF ORIENTED ISOTACTIC POLYPROPYLENE WITH MOLECULAR RESOLUTION
    SNETIVY, D
    GUILLET, JE
    VANCSO, GJ
    POLYMER, 1993, 34 (02) : 429 - 431
  • [33] Image Calculations with a Numerical Frequency-Modulation Atomic Force Microscope
    Castanie, F.
    Nony, L.
    Gauthier, S.
    Bouju, X.
    JOURNAL OF PHYSICAL CHEMISTRY C, 2013, 117 (20): : 10492 - 10501
  • [34] Modification of a commercial atomic force microscopy for low-noise, high-resolution frequency-modulation imaging in liquid environment
    Rode, S.
    Stark, R.
    Luebbe, J.
    Troeger, L.
    Schuette, J.
    Umeda, K.
    Kobayashi, K.
    Yamada, H.
    Kuehnle, A.
    REVIEW OF SCIENTIFIC INSTRUMENTS, 2011, 82 (07):
  • [35] Frequency noise in frequency modulation atomic force microscopy
    Kobayashi, Kei
    Yamada, Hirofumi
    Matsushige, Kazumi
    REVIEW OF SCIENTIFIC INSTRUMENTS, 2009, 80 (04):
  • [36] Water and 2-Propanol Structured on Calcite (104) Probed by Frequency-Modulation Atomic Force Microscopy
    Imada, Hirotake
    Kimura, Kenjiro
    Onishi, Hiroshi
    LANGMUIR, 2013, 29 (34) : 10744 - 10751
  • [37] Increasing the Q factor in the constant-excitation mode of frequency-modulation atomic force microscopy in liquid
    Ebeling, D.
    Hoelscher, H.
    Anczykowski, B.
    APPLIED PHYSICS LETTERS, 2006, 89 (20)
  • [38] Simulated measurement of small metal clusters by frequency-modulation non-contact atomic force microscopy
    Fain, SC
    Polwarth, CA
    Tait, SL
    Campbell, CT
    French, RH
    NANOTECHNOLOGY, 2006, 17 (07) : S121 - S127
  • [39] In situ atomic force microscopy of the mesomorphic - Monoclinic phase transition in isotactic polypropylene
    Androsch, Rene
    MACROMOLECULES, 2008, 41 (03) : 533 - 535
  • [40] Molecular resolution investigation of tetragonal lysozyme (110) face in liquid by frequency-modulation atomic force microscopy
    Nagashima, Ken
    Abe, Masayuki
    Morita, Seizo
    Oyabu, Noriaki
    Kobayashi, Kei
    Yamada, Hirofumi
    Ohta, Masahiro
    Kokawa, Ryohei
    Murai, Ryota
    Matsumura, Hiroyoshi
    Adachi, Hiroaki
    Takano, Kazufumi
    Murakami, Satoshi
    Inoue, Tsuyoshi
    Mori, Yusuke
    JOURNAL OF VACUUM SCIENCE & TECHNOLOGY B, 2010, 28 (03):
12345