3-Ethynyl-2,2,5,5-tetramethyl-1-oxyl-3-pyrroline

被引：2
|
作者：
Frolow, Olga [1 ]
Bats, Jan W. [1 ]
Engels, Joachim W. [1 ]
机构：
[1] Goethe Univ Frankfurt, Inst Organ Chem, D-60438 Frankfurt, Germany
来源：
ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE | 2009年 / 65卷
关键词：
D O I：
10.1107/S1600536809026725
中图分类号：
O7 [晶体学];
学科分类号：
0702 ; 070205 ; 0703 ; 080501 ;
摘要：
The five-membered ring of the title compound, C10H14NO, is almost planar [mean deviation from best plane = 0.006 (1) angstrom]. The N-O bond is in the plane of the five-membered ring. The molecule is positioned about a pseudo-mirror plane at y = 0.375. In the crystal, molecules are connected by intermolecular C-H center dot center dot center dot O contacts into layers parallel to (010).
引用
收藏
页码：O1848 / U2891
页数：9
相关论文
共 50 条
  • [31] Modification of surface lysine residues in immunoglobulin G by spin-label 2,2,5,5-tetramethyl-3-maleimidopyrrolidine-1-oxyl
    Lapuk, VA
    Varlamova, EY
    Mozoleva, AP
    Anisimov, NV
    Timofeev, VP
    BIOFIZIKA, 1999, 44 (05): : 806 - 810
  • [32] CRYSTALLOGRAPHIC STRUCTURES OF RACEMIC AND OPTICALLY-ACTIVE FORMS OF 2,2,5,5-TETRAMETHYL PYRROLIDINE-3-CARBOXAMIDE-1-OXYL
    CHION, B
    LAJZEROWICZ, J
    ACTA CRYSTALLOGRAPHICA SECTION B-STRUCTURAL SCIENCE, 1975, 31 (MAY15): : 1430 - 1435
  • [33] Oxidation of 1,3-dioxacyclanes with oxone and potassium persulfate catalyzed by 2,2,5,5-tetramethyl-4-phenyl-3-imidazoline-3-oxide-1-oxyl
    Akbalina, ZF
    Kabalnova, NN
    Zlotsky, SS
    Grigoriev, IA
    Shereshovets, VV
    Tolstikov, GA
    REACTION KINETICS AND CATALYSIS LETTERS, 2001, 72 (01): : 147 - 152
  • [34] INTRAMOLECULAR SPIN EXCHANGE AND STRUCTURE OF PALLADIUM(II) COMPLEXES WITH 2,2,5,5-TETRAMETHYL-4-THIOXO-3-IMIDAZOLIDINE-1-OXYL
    EVSTIFEROV, MV
    VANIFATOVA, NG
    PETRUKHIN, OM
    KOKORIN, AI
    VOLODARSKII, LB
    BULLETIN OF THE ACADEMY OF SCIENCES OF THE USSR DIVISION OF CHEMICAL SCIENCE, 1988, 37 (11): : 2241 - 2246
  • [35] Crystal structure of copper(II) and cobalt(II) hexafluoroacetylacetonate comtlexes with 2,2,5,5-tetramethyl-4-prenyl-3-imidazoline-1-oxyl-3-oxide
    Burdukov, AB
    Pervukhina, NV
    Ovcharenko, VI
    JOURNAL OF STRUCTURAL CHEMISTRY, 2001, 42 (05) : 826 - 832
  • [36] Oxidation of 1,3-Dioxacyclanes with Oxone and Potassium Persulfate Catalyzed by 2,2,5,5-Tetramethyl-4-Phenyl-3-Imidazoline-3-Oxide-1-Oxyl
    Z.F. Akbalina
    N.N. Kabalnova
    S.S. Zlotsky
    I.A. Grigoriev
    V.V. Shereshovets
    G.A. Tolstikov
    Reaction Kinetics and Catalysis Letters, 2001, 72 : 147 - 152
  • [37] Crystal Structure of Copper(II) and Cobalt(II) Hexafluoroacetylacetonate Complexes with 2,2,5,5-Tetramethyl-4-phenyl-3-imidazoline-1-oxyl-3-oxide
    A. B. Burdukov
    N. V. Pervukhina
    V. I. Ovcharenko
    Journal of Structural Chemistry, 2001, 42 : 826 - 832
  • [38] CRYSTAL AND MOLECULAR-STRUCTURE OF CATENA-(BIS(HEXAFLUOROACETYLACETONATO) COPPER(II)-MU-[4-ISOPROPYL-2,2,5,5-TETRAMETHYL-1-OXYL-3-IMIDAZOLINE-(O,N-3)-(HEXAFLUOROACETYLACETONATO)COPPER(I)-4-ISOPROPYL-2,2,5,5-TETRAMETHYL-1-OXYL-3-IMIDAZOLINE-(N-3,O)])
    PERVUKHINA, NV
    PODBEREZSKAYA, NV
    JOURNAL OF STRUCTURAL CHEMISTRY, 1994, 35 (03) : 399 - 403
  • [39] Studies on the Solvent Effect of N-Carbamoyl-N-(1-Oxyl 2,2,5,5-Tetramethyl-Pyrrolin-3-yl) Ureas
    Zhang Ziyi and Wei Lulin (Department of Chemistry
    Chemical Journal of Chinese Universities, 1990, (01) : 20 - 27
  • [40] RADICAL REAGENTS IN ELECTRON-SPIN-RESONANCE ELEMENT DETERMINATION - 2,2,5,5-TETRAMETHYL-4-THION-3-IMIDAZOLIDINE-1-OXYL
    VANIFATOVA, NG
    EVSTIFEROV, MV
    MARTIN, VV
    PETRUKHIN, OM
    VOLODARSKII, LB
    ZOLOTOV, YA
    JOURNAL OF ANALYTICAL CHEMISTRY OF THE USSR, 1988, 43 (03): : 341 - 345
12345