Two novel Pb(II)-organic frameworks based on polycarboxylate ligands: Syntheses, structures, and luminescent properties

被引：6

作者：

Zhang, Yanan ^{[1
]}

Dang, Beijun ^{[1
]}

Wang, Yu ^{[2
]}

Huang, Wenhuan ^{[1
]}

Yin, Haiju ^{[1
]}

机构：

[1] Shaanxi Univ Sci & Technol, Coll Chem & Chem Engn, Xian 710021, Shaanxi, Peoples R China

[2] Xian Modern Chem Res Inst, Xian, Shaanxi, Peoples R China

来源：

INORGANIC CHEMISTRY COMMUNICATIONS | 2015年 / 61卷

基金：

中国国家自然科学基金;

关键词：

Pb-II-coordination framework; Organic-acid ligands; Network topology; Fluorescence; METAL-ORGANIC FRAMEWORKS; COORDINATION POLYMERS; OPTICAL-PROPERTIES; CRYSTAL-STRUCTURES; SERIES; ACID; POLYCATENATION; CONSTRUCTION; DIVERSITIES; COMPLEXES;

D O I：

10.1016/j.inoche.2015.08.014

中图分类号：

O61 [无机化学];

学科分类号：

070301 ; 081704 ;

摘要：

Two novel Pb(II) complexes, {[Pb-1.5(BPIC)]center dot 0.25H(2)O) (1) and {[Pb(ADC) center dot (H2O)])(2), (H3BPTC = biphenyl-3,2' 5'-tricarboxylate, H(2)ADC = 1,3-Adamantanedicarboxylic acid) were successfully synthesized through varying the different polycarboxylate ligands. The compounds were structurally characterized by elemental analysis, IR and single-mystal X-ray diffraction. Compound 1 exhibits a 3D porous coordination framework, which possesses a new 3-nodal (5,6,8)-connected topology. Compound 2 shows a two-dimensional layer containing a 1D nanotube structure. In addition, compounds 1 and 2 exhibit high thermal stability and fluorescent properties in the solid state at room temperature. (C) 2015 Elsevier B.V. All rights reserved.

引用

页码：89 / 92

页数：4

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