Modified stepwise method for determining heat capacity by DSC

被引：17
|
作者：
Pilar, Radim [1 ]
Honcova, Pavla [1 ]
Kostal, Petr [1 ]
Sadovska, Galina [1 ]
Svoboda, Ladislav [1 ]
机构：
[1] Univ Pardubice, Dept Inorgan Technol, Pardubice 53210, Czech Republic
来源：
JOURNAL OF THERMAL ANALYSIS AND CALORIMETRY | 2014年 / 118卷 / 01期
关键词：
DSC; Heat capacity; Stepwise method; Continuous method; Accuracy of C-p; THERMODYNAMIC PROPERTIES; THERMAL-PROPERTIES; CALORIMETRY; PRECISION; RANGE;
D O I：
10.1007/s10973-014-3982-1
中图分类号：
O414.1 [热力学];
学科分类号：
摘要：
The methods of heat capacity data determination from differential scanning calorimetry measurements are described. The negative effects increasing uncertainty of heat capacity determination are mentioned. Modified stepwise method was described and verified using molybdenum, copper, and gold standards. Modified stepwise method provides better accuracy of C (p) values compared to continuous and stepwise method.
引用
收藏
页码：485 / 491
页数：7
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