The fcc/bcc phase transition in FexNi100-x nanoparticles resolved by first-order reversal curves

被引:16
|
作者
Mokarian, Mohammad Hossein [1 ]
Almasi-kashi, Mohammad [2 ]
Alikhanzadeh-arani, Sima [1 ]
Ramazani, Abdolali [2 ]
机构
[1] Univ Kashan, Inst Nano Sci & Nano Technol, Kashan 8731751167, Iran
[2] Univ Kashan, Dept Phys, Kashan 8731751167, Iran
关键词
MAGNETIC-PROPERTIES; FECO NANOPARTICLES; PARTICLES; MONODISPERSE; GROWTH; ARRAYS;
D O I
10.1007/s10853-017-1025-6
中图分类号
T [工业技术];
学科分类号
08 ;
摘要
One-pot polyol processing was successfully used for the preparation of FexNi100-x nanoparticles. By increasing Ni concentration in FexNi100-x alloy, the phase transition from bcc to fcc crystalline structure was clearly indicated by the XRD data as well as the measured hysteresis loops. FORC diagrams demonstrated that the prepared samples consist of single-domain magnetic particles with a uniform particle size. By changing the molar ratio of the precursors, different compositions of FeNi alloy were obtained. The influence of the temperature, solvent, surfactant, and amount of NaOH was also studied on the particle size, structure, and magnetic properties of the products.
引用
收藏
页码:7831 / 7842
页数:12
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