One-pot polyol processing was successfully used for the preparation of FexNi100-x nanoparticles. By increasing Ni concentration in FexNi100-x alloy, the phase transition from bcc to fcc crystalline structure was clearly indicated by the XRD data as well as the measured hysteresis loops. FORC diagrams demonstrated that the prepared samples consist of single-domain magnetic particles with a uniform particle size. By changing the molar ratio of the precursors, different compositions of FeNi alloy were obtained. The influence of the temperature, solvent, surfactant, and amount of NaOH was also studied on the particle size, structure, and magnetic properties of the products.
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Univ Washington, Dept Earth & Space Sci, Mineral Phys Grp, Seattle, WA 98195 USAUniv Washington, Dept Earth & Space Sci, Mineral Phys Grp, Seattle, WA 98195 USA
Shaikh, A. M.
Ghose, Subrata
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Univ Washington, Dept Earth & Space Sci, Mineral Phys Grp, Seattle, WA 98195 USAUniv Washington, Dept Earth & Space Sci, Mineral Phys Grp, Seattle, WA 98195 USA
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Univ Versailles, Grp Etude Mat Condensee, CNRS, UMR 8635, F-78035 Versailles, FranceUniv Versailles, Grp Etude Mat Condensee, CNRS, UMR 8635, F-78035 Versailles, France
Linares, Jorge
Varret, Francois
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Univ Versailles, Grp Etude Mat Condensee, CNRS, UMR 8635, F-78035 Versailles, FranceUniv Versailles, Grp Etude Mat Condensee, CNRS, UMR 8635, F-78035 Versailles, France
Varret, Francois
Codjovi, Epiphane
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Univ Versailles, Grp Etude Mat Condensee, CNRS, UMR 8635, F-78035 Versailles, FranceUniv Versailles, Grp Etude Mat Condensee, CNRS, UMR 8635, F-78035 Versailles, France
Codjovi, Epiphane
Slimani, Ahmed
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Univ Versailles, Grp Etude Mat Condensee, CNRS, UMR 8635, F-78035 Versailles, FranceUniv Versailles, Grp Etude Mat Condensee, CNRS, UMR 8635, F-78035 Versailles, France
Slimani, Ahmed
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Tanasa, Radu
Enachescu, Cristian
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机构:
Alexandru Ioan Cuza Univ, Dept Phys, Fac Phys, R-700506 Iasi, RomaniaUniv Versailles, Grp Etude Mat Condensee, CNRS, UMR 8635, F-78035 Versailles, France
Enachescu, Cristian
Stancu, Alexandru
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Alexandru Ioan Cuza Univ, Dept Phys, Fac Phys, R-700506 Iasi, RomaniaUniv Versailles, Grp Etude Mat Condensee, CNRS, UMR 8635, F-78035 Versailles, France
Stancu, Alexandru
Haasnoot, Jaap
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Leiden Univ, Leiden Inst Chem, Gorlaeus Labs, NL-2300 RA Leiden, NetherlandsUniv Versailles, Grp Etude Mat Condensee, CNRS, UMR 8635, F-78035 Versailles, France