Mechanochemical synthesis of γ-Bi2O3

被引：27
|
作者：
Poleti, D
Karanovic, L
Zdujic, M
Jovalekic, E
Brankovic, Z
机构：
[1] Serbian Acad Arts & Sci, Inst Tech Sci, YU-11000 Belgrade, Serbia Monteneg, Serbia
[2] Fac Min & Geol, Crystallog Lab, YU-11000 Belgrade, Serbia Monteneg, Serbia
[3] Fac Technol & Met Belgrade, Dept Gen & Inorgan Chem, YU-11000 Belgrade, Serbia Monteneg, Serbia
[4] Univ Belgrade, Ctr Multidisciplinary Studies, YU-11000 Belgrade, Serbia
来源：
SOLID STATE SCIENCES | 2004年 / 6卷 / 03期
关键词：
gamma-Bi2O3; mechanochemical treatment; ball milling; unit-cell parameters; crystallite size; reaction kinetics;
D O I：
10.1016/j.solidstatesciences.2003.12.003
中图分类号：
O61 [无机化学];
学科分类号：
070301 ; 081704 ;
摘要：
A series of gamma-Bi2O3 phases doped with Zn, Si, Pb and Fe was prepared by mechanochemical treatment of corresponding oxide mixtures with a nominal composition 6Bi(2)O(3) (.) MOx (MOx = ZnO, SiO2, PbO) and 12Bi(2)O(3) (.) Fe2O3 using high-energy ball mill. The products are characterized by X-ray powder diffraction technique. Influence of milling conditions: milling time from 5 min to 10 h, milling medium (steel or ZrO2) and injected mechanical power on unit-cell parameters and crystallinity of products, as well as on reaction kinetics are investigated and discussed. (C) 2003 Elsevier SAS. All rights reserved.
引用
收藏
页码：239 / 245
页数：7
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