(9E)-9-Benzylidene-2-methylsulfanyl-5-phenyl-6,7,8,9-tetrahydropyrimido[4,5-b]quinolin-4(3H)-one: a hydrogen-bonded R22(8) dimer

被引：0

作者：

Becerra, Diana ^{[1
]}

Insuasty, Braulio ^{[1
]}

Cobo, Justo ^{[2
]}

Glidewell, Christopher ^{[3
]}

机构：

[1] Univ Valle, Dept Quim, Cali, Colombia

[2] Univ Jaen, Dept Quim Inorgan & Organ, Jaen 23071, Spain

[3] Univ St Andrews, Sch Chem, St Andrews KY16 9ST, Fife, Scotland

来源：

ACTA CRYSTALLOGRAPHICA SECTION C-CRYSTAL STRUCTURE COMMUNICATIONS | 2013年 / 69卷

关键词：

crystal structure; hydrogen-bonded dimer; tetrahydropyrimidin-4(3H)-one; biological activity; POTENTIAL ANTITUMOR-ACTIVITY; INTRAMOLECULAR MOTIONS; ANTIMICROBIAL ACTIVITY; CP/MAS NMR; BROMIDES; AGENTS;

D O I：

10.1107/S010827011303059X

中图分类号：

O6 [化学];

学科分类号：

0703 ;

摘要：

In the molecule of the title compound, C25H21N3OS, which was prepared by mild oxidation of the corresponding 5,6,7,8,9,10-hexahydro analogue, the fused carbocyclic ring adopts an envelope conformation. Pairs of molecules are linked into cyclic centrosymmetric dimers by pairs of inversion-related N-H center dot center dot center dot O hydrogen bonds.

引用

页码：1524 / +

页数：9

共 50 条

[31] Crystal structure and computational study of 3,4-dihydroxy-3-hydroxymethyl-9-methyl-6-methylidene-3a, 4,5,6,6a, 9,9a, 9b-octahydroazuleno[4,5-b]furan-2,8(3H,7H)-dione
Celik, Ismail
Akkurt, Mehmet
Aksit, Huseyin
Erenler, Ramazan
Garcia-Granda, Santiago
ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2015, 71 : 1425 - +
[32] 5-BENZYLIDENE-1,2,3,4,4A,5,6,7,8,9A-DECAHYDRO-4A-MORPHOLINO-9-PHENYLXANTHENE, C30H35NO2 (DBM), AND 5-BENZYLIDENE-1,2,3,4,4A,5,6,7,8,9A-DECAHYDRO-9-PHENYL-4A-PIPERIDINOXANTHENE, C31H37NO (DBP)
PONNUSWAMY, MN
TROTTER, J
ACTA CRYSTALLOGRAPHICA SECTION C-CRYSTAL STRUCTURE COMMUNICATIONS, 1984, 40 (MAR) : 511 - 514
[33] HETEROANALOGUES OF ALLOXAZINES .2. STRUCTURE AND TAUTOMERISM OF 6,8-DIMETHYL-7,9-DIOXO-5H-6,7,8,9-TETRAHYDRODIPYRIMIDO[4,5-B][4',5'-E][1,4]THIAZINES
SOLOVEVA, NP
ANISIMOVA, OS
SHEINKER, YN
NEMERYUK, MP
TRAVEN, NI
ARUTYUNYAN, TG
SHATUHINA, EA
SAFONOVA, TS
KHIMIYA GETEROTSIKLICHESKIKH SOEDINENII, 1992, (10): : 1426 - 1432
[34] Conformational and configurational disorder in 6-(3,4,5-trimethoxyphenyl)-6,7-dihydro-5H-1,3-dioxolo[4,5-g]quinolin-8(5H)-one and 6-(1,3-benzodioxol-5-yl)-6,7-dihydro-5H-1,3-dioxolo[4,5-g]quinolin-8-one: a hydrogen-bonded chain of rings and π-stacked hydrogen-bonded chains
Cuervo, Paola
Abonia, Rodrigo
Cobo, Justo
Glidewell, Christopher
ACTA CRYSTALLOGRAPHICA SECTION C-STRUCTURAL CHEMISTRY, 2009, 65 : O326 - O330
[35] SYNTHESES OF 3,4-DIHYDRO-2H-PYRIDAZINO[4,5-B]-1,4-THIAZIN-8(7H)-ONE AND 5(6H)-ONE
MATSUO, T
TSUKAMOTO, Y
TAKAGI, T
YAGINUMA, H
CHEMICAL & PHARMACEUTICAL BULLETIN, 1982, 30 (03) : 1030 - 1032
[36] 3,7,7-trimethyl-4-phenyl-4,7,8,9-tetrahydro-2H-pyrazolo[3,4-b]quinolin-5-(6H)-one
Cannon, D
Quesada, A
Quiroga, J
Mejía, D
Insuasty, B
Abonia, R
Cobo, J
Nogueras, M
Sánchez, A
Low, JN
ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2001, 57 : o157 - o159
[37] 6,7,8,9,10,11,12,13-Octahydro-5H-1,3-dithiole[4,5-b][1,4]dithiacyclotridecine-2-thione
Heshmatpour, Felora
Darviche, Fatemeh
Emdadi, Zeynab
Neumueller, Bernhard
ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2008, 64 : O402 - U1979
[38] 4-PHENYL-6,7,8,9-TETRAHYDRO-[1]BENZOTHIENO[3,2-E][1,2,4]TRIAZOLO[4,3-A]PYRIMIDIN-5(4H)-ONE
VELAVAN, R
SIVAKUMAR, K
PATHAK, US
JAIN, KS
SINGH, S
FUN, HK
ACTA CRYSTALLOGRAPHICA SECTION C-CRYSTAL STRUCTURE COMMUNICATIONS, 1995, 51 : 2092 - 2094
[39] Synthesis, Characterization and Biological Activity of (E)-9-Benzylidene-5-phenyl-5,6,7,8,9,10-hexahydro-[1,2,4]triazolo [3,4-a]quinazoline
Almutaleb, Arabya A. A.
Alrawaig, Nadia S.
Saad, Alanaq M.
Shamsi, Shamsi S.
JORDAN JOURNAL OF CHEMISTRY, 2020, 15 (03) : 111 - 118
[40] 2-Amino-9-aryl-3-cyano-4-methyl-7-oxo-6,7,8,9-tetrahydropyrido[2′,3′:4,5]thieno[2,3-b]pyridine derivatives as selective progesterone receptor agonists
Wang, Yonghui
Duraiswami, Chaya
Madauss, Kevin P.
Tran, Thuy B.
Williams, Shawn P.
Deng, Su-Jun
Graybill, Todd L.
Hammond, Marlys
Jones, David G.
Grygielko, Eugene T.
Bray, Jeffrey D.
Thompson, Scott K.
BIOORGANIC & MEDICINAL CHEMISTRY LETTERS, 2009, 19 (17) : 4916 - 4919

← 1 2 3 4 5 →