Determination of tylosin in milk by reversed-phase liquid chromatography

被引：0
|
作者：
Usleber, E [1 ]
Straka, M [1 ]
Martlbauer, E [1 ]
机构：
[1] UNIV MUNICH,FAC VET,INST HYG & TECHNOL FOOD ANIM ORIGIN,D-80539 MUNICH,GERMANY
来源：
ARCHIV FUR LEBENSMITTELHYGIENE | 1997年 / 48卷 / 04期
关键词：
D O I：
暂无
中图分类号：
O69 [应用化学];
学科分类号：
081704 ;
摘要：
A method for the determination of tylosin in milk is reported. Milk samples were defatted, diluted with water and purified using RP18 solid phase extraction columns. Determination was achieved by reversed-phase liquid chromatography and UV detection at 287 nm. Peak identity was checked by recording the UV spectrum. Detection limit for tylosin in milk was 12.5-15 ng/ml. Recoveries for tylosin from spiked milk samples (concentration range: 25-100 ng/ml) were 81.7-87.6%, with coefficients of variation of 7.32-17.1%.
引用
收藏
页码：75 / 76
页数：2
相关论文
共 50 条
  • [21] Improving reversed-phase liquid chromatography
    Jackson, PT
    Carr, PW
    CHEMTECH, 1998, 28 (10) : 29 - 37
  • [22] Phase collapse in reversed-phase liquid chromatography
    Majors, RE
    LC GC NORTH AMERICA, 2002, 20 (06) : 516 - +
  • [23] DETERMINATION OF FUROSINE IN PASTEURIZED MILK BY USE OF ION-PAIR REVERSED-PHASE LIQUID-CHROMATOGRAPHY
    CLAWINRADECKER, I
    SCHLIMME, E
    KIELER MILCHWIRTSCHAFTLICHE FORSCHUNGSBERICHTE, 1995, 47 (02): : 169 - 175
  • [24] Determination of four fluoroquinolones in milk by on-line immunoaffinity capture coupled with reversed-phase liquid chromatography
    Holtzapple, CK
    Buckley, SA
    Stanker, LH
    JOURNAL OF AOAC INTERNATIONAL, 1999, 82 (03) : 607 - 613
  • [25] Determination of four fluoroquinolones in milk by on-line immunoaffinity capture coupled with reversed-phase liquid chromatography
    Holtzapple, Carol K.
    Buckley, Sandra A.
    Stanker, Larry H.
    Journal of AOAC International, 82 (03): : 607 - 613
  • [26] Strategies for the determination of the volume and composition of the stationary phase in reversed-phase liquid chromatography
    Wang, Mei
    Mallette, Jennifer
    Parcher, Jon F.
    JOURNAL OF CHROMATOGRAPHY A, 2008, 1190 (1-2) : 1 - 7
  • [27] Comparison of Micellar and Reversed-Phase Liquid Chromatography for Determination of Sulfamethoxazole and Trimethoprim
    A. U. Kulikov
    A. G. Verushkin
    L. P. Loginova
    Chromatographia, 2005, 61 : 455 - 463
  • [28] Simultaneous determination of metformin in combination with rosiglitazone by reversed-phase liquid chromatography
    Kolte, BL
    Raut, BB
    Deo, AA
    Bagool, MA
    Shinde, DB
    JOURNAL OF CHROMATOGRAPHIC SCIENCE, 2004, 42 (02) : 70 - 73
  • [29] Determination of the pH of binary mobile phases for reversed-phase liquid chromatography
    Rosés, M
    JOURNAL OF CHROMATOGRAPHY A, 2004, 1037 (1-2) : 283 - 298
  • [30] Determination of lipid profile in meningococcal polysaccharide reversed-phase liquid chromatography
    Li, Y
    Lander, R
    Manger, W
    Lee, A
    JOURNAL OF CHROMATOGRAPHY B-ANALYTICAL TECHNOLOGIES IN THE BIOMEDICAL AND LIFE SCIENCES, 2004, 804 (02): : 353 - 358
12345