Determination of tylosin in milk by reversed-phase liquid chromatography

被引：0
|
作者：
Usleber, E [1 ]
Straka, M [1 ]
Martlbauer, E [1 ]
机构：
[1] UNIV MUNICH,FAC VET,INST HYG & TECHNOL FOOD ANIM ORIGIN,D-80539 MUNICH,GERMANY
来源：
ARCHIV FUR LEBENSMITTELHYGIENE | 1997年 / 48卷 / 04期
关键词：
D O I：
暂无
中图分类号：
O69 [应用化学];
学科分类号：
081704 ;
摘要：
A method for the determination of tylosin in milk is reported. Milk samples were defatted, diluted with water and purified using RP18 solid phase extraction columns. Determination was achieved by reversed-phase liquid chromatography and UV detection at 287 nm. Peak identity was checked by recording the UV spectrum. Detection limit for tylosin in milk was 12.5-15 ng/ml. Recoveries for tylosin from spiked milk samples (concentration range: 25-100 ng/ml) were 81.7-87.6%, with coefficients of variation of 7.32-17.1%.
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页码：75 / 76
页数：2
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